苯乙烯-α, β, β-d3合成路线 (共 11 条)
反应条件
RuHCl(CO)(PPh3)3; water-d2 in 1,4-dioxane
T=100°C; 1 h;
参考文献
Tse, Sunny Kai San; Xue, Peng; Lin, Zhenyang; Jia, Guochen
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 9 p. 1512 - 1522
反应条件
in cyclohexane
T=20°C; Flash photolysis;
参考文献
Zhang, Yunlong; Kubicki, Jacek; Platz, Matthew S.
Organic Letters, 2010 , vol. 12, # 14 p. 3182 - 3184
反应条件
ruthenium(II)-carbonyl-tris(triphenylphosphine) dihydride in 3,3-dimethyl-butan-2-one
T=120°C; 0.0833333 h; Sealed tube;
参考文献
Hiroshima, Shun; Matsumura, Daiki; Kochi, Takuya; Kakiuchi, Fumitoshi
Organic Letters, 2010 , vol. 12, # 22 p. 5318 - 5321
反应条件
T=390°C; Irradiationflash vacuum thermolysis; Yield given;
参考文献
Chapman, Orville L.; Johnson, Jeffery W.; Mahon, Robert J. Mc; West, Paul R.
Journal of the American Chemical Society, 1988 , vol. 110, # 2 p. 501 - 509
反应条件
deuterium; palladium(0) bis(p-tolylimino)acenaphthene dimethylfumaric acid
参考文献
Harthun, Andreas; Giernoth, Ralf; Elsevier, Cornelis J.; Bargon, Joachim
Chemical Communications, 1996 , # 21 p. 2483 - 2484
反应条件
[(.eta.6-benzene)(PCy3)(CO)RuD]BF4 in dichloromethane
T=20°C; 0.5 h;
参考文献
Lee, Do W.; Yi, Chae S.
Organometallics, 2010 , vol. 29, # 15 p. 3413 - 3417
反应条件
in various solvent(s)
T=-258.2°C; Irradiationλ > 470 nm; var. solv.: xenon, var. temp; Rate constantProduct distribution;
参考文献
McMahon, Robert J.; Chapman, Orville L.
Journal of the American Chemical Society, 1987 , vol. 109, # 3 p. 683 - 692
反应条件
[(tris[2-(diisopropylphosphino)phenyl]borane)Fe(N2)]; deuterium
P=760.051 Torr; Inert atmosphere;
参考文献
Fong, Henry; Moret, Marc-Etienne; Lee, Yunho; Peters, Jonas C.
Organometallics, 2013 , vol. 32, # 10 p. 3053 - 3062
反应条件
T=470°C; Irradiationflash vacuum thermolysis; Yield given. Yields of byproduct given;
参考文献
Chapman, Orville L.; Johnson, Jeffery W.; Mahon, Robert J. Mc; West, Paul R.
Journal of the American Chemical Society, 1988 , vol. 110, # 2 p. 501 - 509
参考文献
Wall; Brown
Journal of Physical Chemistry, 1957 , vol. 61, p. 129,131