反应条件
t-BuLi in tetrahydrofuran; pentane
byproducts: LiBr, LiCl, Me2CCH2; Ar; pentane soln. of BuLi (2.25 mmol) added to THF soln. of Sn compd. (0.64 mmol) at -78°C, mixt. stirred for 15 min, THF soln. of (p-MeO)2SnCl2 (0.68 mmol) added, mixt. warmed to room temp.; evapd., WCC(hexane/ethyl acetate=5/1), elem. anal.;
参考文献
Saito, Masaichi; Imaizumi, Sanae; Tajima, Tomoyuki
European Journal of Inorganic Chemistry, 2010 , # 14 p. 2153 - 2157
