in tetrahydrofuran; benzene
(N2); SnCl4 was added to cooled and stirred Grignard soln., prepd. from p-bromoanisole and Mg in THF, and refluxed for 1 h; filtered soln. was evapd. in vac. and pptd. with acetone, crude product was dissolved in benzene and pptd. with EtOH; recrystn. from EtOH; elem. anal.;
参考文献
Wharf, Ivor; Simard, Michael G.
Journal of Organometallic Chemistry, 1987 , vol. 332, p. 85 - 94
in not given
Kocheshkov redistribution reaction (K. A. Kocheshkov, M. M. Nadi and A. P. Aleksandrov Chem. Ber. 67 (1934) 1348; recrystn. from hexane, elem. anal.;
