1,1,3,3,3-五氟-2-三氟甲基丙基甲基醚合成路线 （共 17 条）
参考文献
Knunjanz et al.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1956 , p. 1353,1360;engl.Ausg.S.1387,1393
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Koshar et al.
Journal of the American Chemical Society, 1957 , vol. 79, p. 1741,1742
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Inouye, Yoshio; Yokozawa, Tsutomu; Ishikawa, Nobuo
Journal of Fluorine Chemistry, 1985 , vol. 27, p. 379 - 384
反应条件
sodium hydride in N,N-dimethyl-formamide Ambient temperaturedifferent solvents and bases;
参考文献
Inouye,Y.; Higuchi,Y.
Journal of Fluorine Chemistry, 1985 , vol. 27, p. 231
反应条件
analoge Reaktion mit Aethanol;
参考文献
Knunjanz et al.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1956 , p. 1353,1360;engl.Ausg.S.1387,1393
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Koshar et al.
Journal of the American Chemical Society, 1957 , vol. 79, p. 1741,1742
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Brice et al.
Journal of the American Chemical Society, 1953 , vol. 75, p. 2698,2702
反应条件
calcium hydroxide powder; N-benzyl-N,N,N-triethylammonium chloride in water
参考文献
Journal of Fluorine Chemistry, , vol. 27, p. 231
反应条件
potassium hydroxide T=65 - 80°C; 1.5 h; var. reag.: NaOH, Ca(OH)2;
参考文献
Journal of Fluorine Chemistry, , vol. 29, p. 471 - 475
反应条件
sulfuric acid; silica gel T=65 - 90°C; 1 h;
参考文献
Misaki, Susumu; Takamatsu, Shuichi
Journal of Fluorine Chemistry, 1984 , vol. 24, p. 531 - 534
反应条件
Yield given. Multistep reaction;
参考文献
Yokozawa, Tsutomu; Nakai, Takeshi; Ishikawa, Nobuo
Tetrahedron Letters, 1984 , vol. 25, # 36 p. 3987 - 3990
反应条件
sulfuric acid; triethylamine 1.) DMF, from 10 to 20 deg C, 2.) ether, RT, overnight; Yield given. Multistep reaction;
参考文献
Ishikawa, Nobuo; Yokozawa, Tsutomu
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 3 p. 724 - 726
反应条件
SbF5 in neat (no solvent)
参考文献
England, David C.
Journal of Organic Chemistry, 1984 , vol. 49, # 21 p. 4007 - 4008
反应条件
triethylamine in N,N-dimethyl-formamide 1.) 20-25 deg C, 1 h; 2.) 45-70 deg C, 1 h;
参考文献
Journal of Fluorine Chemistry, , vol. 35, p. 275
