(R)-(+)-N-苄基-1-苯乙胺合成路线 （共 41 条）
反应条件
in tetrahydrofuran T=20°C; 16 h;
参考文献
Plaquevent, Jean-Christophe; Ravard, Alain
Journal of Organometallic Chemistry, 1989 , vol. 361, p. C51 - C53
反应条件
1: 56 percent / m-CPBA / CH2Cl2 2: ethanol / 72 h / 80 °C 3: Raney Nickel / ethanol / 3 h View Scheme
参考文献
Pyne, Stephen G.; Bloem, Peter; Griffith, Renate
Tetrahedron, 1989 , vol. 45, # 22 p. 7013 - 7022
反应条件
1: 41 percent / heptane / 120 h / Ambient temperature 2: 56 percent / m-CPBA / CH2Cl2 3: ethanol / 72 h / 80 °C 4: Raney Nickel / ethanol / 3 h View Scheme
参考文献
Pyne, Stephen G.; Bloem, Peter; Griffith, Renate
Tetrahedron, 1989 , vol. 45, # 22 p. 7013 - 7022
反应条件
1: 89 percent / manganese dioxide / CH2Cl2 / Heating 2: 78 percent / sodium borohydride / methanol / 0.33 h / 0 °C View Scheme
参考文献
Blackburn, Leonie; Taylor, Richard J. K.
Organic Letters, 2001 , vol. 3, # 11 p. 1637 - 1639
反应条件
1,4-diaza-bicyclo[2.2.2]octane; [RuCl2(IiPr)(p-cymene)] in toluene 24 h; Inert atmosphereMolecular sieveReflux;
参考文献
Maggi, Agnese; Madsen, Robert
Organometallics, 2012 , vol. 31, # 1 p. 451 - 455
反应条件
W-2 Raney nickel in diethyl ether; water 1 h;
参考文献
Pyne, Stephen G.; Bloem, Peter; Chapman, Sandra L.; Dixon, Christine E.; Griffith, Renate
Journal of Organic Chemistry, 1990 , vol. 55, # 3 p. 1086 - 1093
反应条件
1: ethanol / 3 h / Heating 2: 184 g / NaBH4 / 72 h / 20 °C View Scheme
参考文献
Bunnage, Mark E.; Davies, Stephen G.; Parkin, Richard M.; Roberts, Paul M.; Smith, Andrew D.; Withey, Jonathan M.
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 22 p. 3337 - 3354
反应条件
nickel in ethanol 3 h;
参考文献
Pyne, Stephen G.; Bloem, Peter; Griffith, Renate
Tetrahedron, 1989 , vol. 45, # 22 p. 7013 - 7022
反应条件
1: ethanol / 72 h / 80 °C 2: Raney Nickel / ethanol / 3 h View Scheme
参考文献
Pyne, Stephen G.; Bloem, Peter; Griffith, Renate
Tetrahedron, 1989 , vol. 45, # 22 p. 7013 - 7022
反应条件
1: toluene / 24 h / 20 °C / |Inert atmosphere; |Molecular sieve 2: benzo[1,3,2]dioxaborole; 1,1,1-trifluoro-N-(4-oxido-2,6-bis(2,4,6-triisopropylphenyl)dinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepin-4-yl)methanesulfonamide / pentane / 24 h / -78 - -22 °C / |Inert atmosphere; |Schlenk technique View Scheme
参考文献
Hermeke, Julia; Mewald, Marius; Oestreich, Martin
Journal of the American Chemical Society, 2013 , vol. 135, # 46 p. 17537 - 17546
