N-(2-甲氧基乙基)甲基胺合成路线 (共 9 条)
反应条件
hydrogen; palladium on activated charcoal in ethanol T=20°C; 1.5 h;
参考文献
Afonso, Carlos A. M.; Lourenco, Nuno M. T.; De Rosatella, Andreia A.
Molecules, 2006 , vol. 11, # 1 p. 81 - 102
参考文献
Alanine, Alexander; Flohr, Alexander; Miller, Aubry Kern; Norcross, Roger David; Riemer, Claus
Patent: US2002/45615 A1, 2002 ;
参考文献
Alanine, Alexander; Flohr, Alexander; Miller, Aubry Kern; Norcross, Roger David; Riemer, Claus
Patent: US2002/45615 A1, 2002 ;
反应条件
in ethanol T=74°C; 23 h;
参考文献
Heathcote, Robert; Howell, James A. S.; Jennings, Nicola; Cartlidge, David; Cobden, Lisa; Coles, Simon; Hursthouse, Michael
Dalton Transactions, 2007 , # 13 p. 1309 - 1315
反应条件
sodium hydride in hexane; diethylene glycol dimethyl ether 1.) 40 deg C, 6 h, 2.) 12 h, r.t.;
参考文献
Bettermann, Gerhard; Schomburg, Dietmar; Schmutzler, Reinhard
Phosphorus and Sulfur and the Related Elements, 1986 , vol. 28, p. 327 - 336
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Mndshojan et al.
Doklady Akademii Nauk Armyanskoi SSR, 1958 , vol. 27, p. 179,182
Chem.Abstr., 1960 , p. 22475
反应条件
sodium hydride 1.) THF, room temp., 1 h; 2.) room temp., 1 h; Yield given. Multistep reaction;
参考文献
Kashima, Choji; Harada, Kazuo; Omote, Yoshimori
Canadian Journal of Chemistry, 1985 , vol. 63, p. 288 - 290
反应条件
perchloric acid T=10.1°C; ΔH(excit.); -ΔS(excit.); acidity and solvent deuterium isotope effects; different temperatures; KineticsThermodynamic data;
参考文献
Pihlaja, Kalevi; Parkkinen, Aija; Loennberg, Harri
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , p. 1223 - 1226
反应条件
formic acid in water Eschweiler-Clarke reaction; 16 h; Heating;
参考文献
Bilke, Julia L.; O'Brien, Peter
Journal of Organic Chemistry, 2008 , vol. 73, # 16 p. 6452 - 6454