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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
38262-42-9
合成路线
（共 24 条）
38262-42-9
→
反应条件
166328-07-0
(1-萘)三氟硼酸钾
反应条件
1: With tetrahydroxydiboron; [1,3-bis(diphenylphosphino) propane] dichloronickel(II); N-ethyl-N,N-diisopropylamine; triphenylphosphine in ethanol T=50°C; Miyaura Borylation Reaction; 8 h; Inert atmosphereSealed tube; 2: With potassium hydrogen difluoride in methanol; ethanol; water T=0 - 20°C; 0.5 h;
参考文献
Molander, Gary A.; Cavalcanti, Livia N.; Garcia-Garcia, Carolina
Journal of Organic Chemistry, 2013 , vol. 78, # 13 p. 6427 - 6439
38262-42-9
+
74-89-5
甲胺
→
反应条件
2216-68-4
N-甲基-1-萘胺
反应条件
potassium phosphate; [Pd(η3-1-Ph-allyl)(μ-Cl)]2; (Mor-DalPhos) in 1,4-dioxane; tert-butyl alcohol T=110°C; Buchwald-Hartwig Coupling; Inert atmosphereGlovebox; chemoselective reaction;
参考文献
Alsabeh, Pamela G.; Stradiotto, Mark
Angewandte Chemie - International Edition, 2013 , vol. 52, # 28 p. 7242 - 7246
Angew. Chem., 2013 , vol. 125, # 28 p. 7383 - 7387
905966-40-7
+
38262-42-9
→
反应条件
229467-26-9
4-(萘-1-基)苯甲酸甲酯
反应条件
bis(1,5-cyclooctadiene)nickel (0); potassium phosphate; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25°C; 12 h; Inert atmosphere;
参考文献
Leowanawat, Pawaret; Zhang, Na; Percec, Virgil
Journal of Organic Chemistry, 2012 , vol. 77, # 2 p. 1018 - 1025
38262-42-9
+
99768-12-4
4-甲氧羰基苯硼酸
→
反应条件
229467-26-9
4-(萘-1-基)苯甲酸甲酯
反应条件
anhydrous dipotassium phosphate; [1,3-bis(diphenylphosphino) propane] dichloronickel(II) in 1,4-dioxane T=100 - 110°C; Suzuki-Miyaura coupling reaction; Inert atmosphere;
参考文献
Gao, Han; Li, You; Zhou, Yi-Guo; Han, Fu-She; Lin, Ying-Jie
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 2-3 p. 309 - 314
38262-42-9
+
1268340-93-7
(吡啶鎓-1-基甲基)三氟硼酸盐
→
反应条件
6947-74-6
反应条件
potassium phosphate; palladium diacetate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in water; tert-butyl alcohol T=110°C; Csp2-Csp3 Suzuki-Miyaura cross-coupling; 1 h; Inert atmosphereSealed tube;
参考文献
Molander, Gary A.; Beaumard, Floriane
Organic Letters, 2011 , vol. 13, # 5 p. 1242 - 1245
38262-42-9
→
反应条件
93321-11-0
反应条件
[Ni0(1,5-cyclooctadiene)2]; potassium phosphate; PCy3∙HBF4 in water; tert-butyl alcohol T=110°C; Suzuki-Miyaura cross coupling; 4 h; Inert atmosphere;
参考文献
Molander, Gary A.; Beaumard, Floriane
Organic Letters, 2010 , vol. 12, # 18 p. 4022 - 4025
38262-42-9
+
5720-06-9
2-甲氧基苯基硼酸
→
反应条件
93321-11-0
反应条件
anhydrous dipotassium phosphate; [1,3-bis(diphenylphosphino) propane] dichloronickel(II) in 1,4-dioxane T=100 - 110°C; Suzuki-Miyaura coupling reaction; Inert atmosphere;
参考文献
Gao, Han; Li, You; Zhou, Yi-Guo; Han, Fu-She; Lin, Ying-Jie
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 2-3 p. 309 - 314
→
反应条件
56432-18-9
4-萘-1-苯甲醛
反应条件
[Ni0(1,5-cyclooctadiene)2]; potassium phosphate; PCy3∙HBF4 in water; tert-butyl alcohol T=110°C; Suzuki-Miyaura cross coupling; 4 h; Inert atmosphere;
参考文献
Molander, Gary A.; Beaumard, Floriane
Organic Letters, 2010 , vol. 12, # 18 p. 4022 - 4025
38262-42-9
→
反应条件
572-52-1
反应条件
[Ni0(1,5-cyclooctadiene)2]; potassium phosphate; PCy3∙HBF4 in water; tert-butyl alcohol T=110°C; Suzuki-Miyaura cross coupling; 4 h; Inert atmosphere;
参考文献
Molander, Gary A.; Beaumard, Floriane
Organic Letters, 2010 , vol. 12, # 18 p. 4022 - 4025
910251-11-5
甲氧基甲基三氟硼酸钾
+
38262-42-9
→
反应条件
5903-23-1
抑芽醚
反应条件
potassium phosphate; dichloro(cycloocta-1,5-diene)palladium(II); DiPPF in water; tert-butyl alcohol T=110°C; Suzuki-Miyaura cross coupling; 4 h; Inert atmosphere;
参考文献
Molander, Gary A.; Beaumard, Floriane
Organic Letters, 2011 , vol. 13, # 15 p. 3948 - 3951
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