1: ethyl chloro-difluoroacetate With chloro-trimethyl-silane; 1,1-dibromo ethane; zinc in N,N-dimethyl-formamide 2: C5H13NO in N,N-dimethyl-formamide T=60°C; 4 h;
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Bijeire, Laurent; Denier, Colette; Mulliez, Michel; De Lima, Waldir Tavares
Phosphorus, Sulfur and Silicon and the Related Elements, 2007 , vol. 182, # 4 p. 881 - 891
diethyl sulphate; zinc multistep reaction, other DMF activators; Product distributionMechanism;
参考文献
Tsukamoto, Takashi; Kitazume, Tomoya
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 10 p. 1177 - 1182
potassium fluoride; copper(l) iodide in N,N-dimethyl-formamide T=100°C; 10 h;
参考文献
Duan, Jian-Xing; Chen, Quing-Yun
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 6 p. 725 - 730
potassium fluoride; copper(l) iodide in N,N-dimethyl-formamide
T=100°C; 10 h;
参考文献
Duan, Jian-Xing; Chen, Quing-Yun
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 6 p. 725 - 730
