反应条件
1: ethyl-α,α,α-trifluoroacetate With sodium hydride in ethylene glycol dimethyl ether; mineral oil 2: 1-(2-methoxyphenyl)ethanone in ethylene glycol dimethyl ether; mineral oil T=160°C; 0.25 h; Microwave irradiation; 3: With hydrogenchloride in ethylene glycol dimethyl ether; water; mineral oil
参考文献
Pettersson, Martin Youngjin; Johnson, Douglas Scott; Subramanyam, Chakrapani; O'Donnell, Christopher John; Ende, Christopher William Am; Fish, Benjamin Adam; Green, Michael Eric; Mullins, Patrick Bradley; Stiff, Cory Michael; Tran, Tuan Phong; Navaratnam, Thayalan
Patent: US2012/252758 A1, 2012 ;
Location in patent: Page/Page column 22 ;