反应条件
1: ortho-bromo-phenol With n-butyllithium in diethyl ether; hexane T=-25 - 20°C; Inert atmosphere; 2: ethyl-α,α,α-trifluoroacetate in diethyl ether; hexane T=-90 - 20°C; 1.25 h; Inert atmosphere; 3: With hydrogenchloride in diethyl ether; hexane; water T=-5°C;
参考文献
Sevenard, Dmitri V.; Vorobyev, Mikhail; Sosnovskikh, Vyacheslav Ya.; Wessel, Helma; Kazakova, Olesya; Vogel, Vera; Shevchenko, Nikolay E.; Nenajdenko, Valentine G.; Lork, Enno; Roeschenthaler, Gerd-Volker
Tetrahedron, 2009 , vol. 65, # 36 p. 7538 - 7552
