THE BOARD OF TRUSTEES OF THE LELAND STANFORD JUNIOR UNIVERSITY; FRANZINI, Raphael M.; KOOL, Eric Todd
Patent: WO2011/5821 A1, 2011 ;
Location in patent: Page/Page column 48 ;
1: ethyl-α,α,α-trifluoroacetate; 2-amino acetophenone With lithium hydride in tetrahydrofuran 2.5 h; Heating; 2: methyl iodide in tetrahydrofuran 12 h; Heating; Title compound not separated from byproducts;
参考文献
Russian Chemical Bulletin, , vol. 51, # 11 p. 2109 - 2115
1: 1-bromo-3,5-dichloro-benzene With diisobutylaluminium hydride; magnesium in tetrahydrofuran; hexane Reflux; 2: ethyl-α,α,α-trifluoroacetate in tetrahydrofuran; hexane T=0°C; 3: With water; ammonium chloride in tetrahydrofuran; hexane
