N-烯丙基-2,2,2-三氟乙酰胺合成路线 （共 9 条）
参考文献
Dey, Subhakar; Sheppard, Terry L.
Organic Letters, 2001 , vol. 3, # 25 p. 3983 - 3986
反应条件
triethylamine; trichloroacetonitrile; triphenylphosphine in acetonitrile T=20°C; 1 h; Inert atmosphere;
参考文献
Kim, Joong-Gon; Jang, Doo Ok
Tetrahedron Letters, 2010 , vol. 51, # 4 p. 683 - 685
反应条件
in tetrahydrofuran T=0 - 20°C; 0.916667 h;
参考文献
ACUCELA INC.
Patent: WO2009/45479 A1, 2009 ;
Location in patent: Page/Page column 157 ;
反应条件
T=20°C; Cooling with ice;
参考文献
Reddington, Mark V.; Cunninghan-Bryant, Daniel
Tetrahedron Letters, 2011 , vol. 52, # 2 p. 181 - 183
反应条件
2,6-di-tert-butyl-4-methylpyridine in tetrachloromethane T=0 - 25°C; 0.0833333 h;
参考文献
Forbus, T. R.; Taylor, S. L.; Martin, J. C.
Journal of Organic Chemistry, 1987 , vol. 52, # 19 p. 4156 - 4159
反应条件
trifluoroacetic anhydride in pyridine; dichloromethane
参考文献
Pfizer Inc.
Patent: US5686434 A1, 1997 ;
反应条件
in dichloromethane T=20°C; 0.5 h;
参考文献
Zanatta, Nilo; Wouters, Ana D.; Fantinel, Leonardo; Da Silva, Fabio M.; Barichello, Rosemario; Da Silva, Pedro E. A.; Ramos, Daniela F.; Bonacorso, Helio G.; Martins, Marcos A. P.
Synlett, 2009 , # 5 p. 755 - 758
反应条件
sodium tetrachloropalladium (II) in acetate buffer; N,N-dimethyl-formamide T=80°C; Heck reaction; pH=5.2; 2 h;
参考文献
Kim, Hyo-Joong; Kim, Myong Jung; Karalkar, Nilesh; Hutter, Daniel; Benner, Steven A.
Nucleosides, Nucleotides and Nucleic Acids, 2008 , vol. 27, # 1 p. 43 - 56
反应条件
sodium tetrachloropalladium (II) in acetate buffer; N,N-dimethyl-formamide
T=80°C; Heck reaction; pH=5.2; 2 h;
参考文献
Kim, Hyo-Joong; Kim, Myong Jung; Karalkar, Nilesh; Hutter, Daniel; Benner, Steven A.
Nucleosides, Nucleotides and Nucleic Acids, 2008 , vol. 27, # 1 p. 43 - 56
