1-甲基-6-硝基-9H-吡啶并[3,4-b]吲哚合成路线 （共 6 条）
反应条件
hydrogenchloride; water; tin(ll) chloride
参考文献
Snyder et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 219
反应条件
sodium nitrate; trifluoroacetic acid
T=0 - 20°C; 6 h;
参考文献
Song, Hongjian; Liu, Yongxian; Liu, Yuxiu; Wang, Lizhong; Wang, Qingmin
Journal of Agricultural and Food Chemistry, 2014 , vol. 62, # 5 p. 1010 - 1018
参考文献
Snyder et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 219
反应条件
1: cis-maleic acid; palladium on activated charcoal / water / 8 h / |Reflux
2: sodium nitrate; trifluoroacetic acid / 6 h / 0 - 20 °C
View Scheme
参考文献
Song, Hongjian; Liu, Yongxian; Liu, Yuxiu; Wang, Lizhong; Wang, Qingmin
Journal of Agricultural and Food Chemistry, 2014 , vol. 62, # 5 p. 1010 - 1018
反应条件
1.1: sulfuric acid / water / 0.5 h / 20 °C
1.2: 7 h / |Reflux
2.1: cis-maleic acid; palladium on activated charcoal / water / 8 h / |Reflux
3.1: sodium nitrate; trifluoroacetic acid / 6 h / 0 - 20 °C
View Scheme
参考文献
Song, Hongjian; Liu, Yongxian; Liu, Yuxiu; Wang, Lizhong; Wang, Qingmin
Journal of Agricultural and Food Chemistry, 2014 , vol. 62, # 5 p. 1010 - 1018
反应条件
1: SnCl2; water; HCl
2: aqueous HBr; CuBr / Diazotization
View Scheme
参考文献
Snyder et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 219
