1-(4-甲氧基苯基)-2-硝基乙醇合成路线 (共 12 条)
参考文献
Groszek
Organic Preparations and Procedures International, 2010 , vol. 42, # 4 p. 373 - 378
反应条件
vinyl acetate; Pseudomonas fluorescens amino lipase in hexane; toluene T=30°C; 48 h; Title compound not separated from byproducts;
参考文献
Borah, Jagat C.; Boruwa, Joshodeep; Kalita, Biswajit; Hazarika, Ajit K.; Barua, Nabin C.
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2005 , vol. 44, # 9 p. 1961 - 1965
反应条件
triethylsilane; trifluoroacetic acid T=0 - 20°C; 1 h;
参考文献
Luzzio, Frederick A.; Wlodarczyk, Marek T.; Duveau, Damien Y.; Chen, Juan
Tetrahedron Letters, 2007 , vol. 48, # 38 p. 6704 - 6708
反应条件
P(i-PrNCH2CH2)3N; magnesium sulfate
0.666667 h; Ambient temperature;
参考文献
Kisanga, Philip B.; Verkade, John G.
Journal of Organic Chemistry, 1999 , vol. 64, # 12 p. 4298 - 4303
反应条件
ammonium acetate
T=90°C; Henry reaction; 0.416667 h; Microwave irradiation;
参考文献
Rodriguez, Jose M.; Dolors Pujol
Tetrahedron Letters, 2011 , vol. 52, # 21 p. 2629 - 2632
反应条件
scandium tris(trifluoromethanesulfonate) in tetrahydrofuran; hexane
T=-78°C; Mukaiyama nitro-aldol reaction; 72 h; Inert atmosphere;
参考文献
MacDonald, Frank K.; Carneiro, Karina M.M.; Pottie, Ian R.
Tetrahedron Letters, 2011 , vol. 52, # 8 p. 891 - 893
反应条件
potassium carbonate; dimethyl sulfate in water; N,N-dimethyl-formamide
参考文献
SmithKline Beckman Corporation
Patent: US4705862 A1, 1987 ;
反应条件
indium in tetrahydrofuran
T=20°C; 4 h; Sonication;
参考文献
Soengas, Raquel G.; Estevez, Amalia M.
European Journal of Organic Chemistry, 2010 , # 27 p. 5190 - 5196
参考文献
Boileau
Bulletin de la Societe Chimique de France, 1953 , p. 1007
反应条件
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in ethyl acetate
RefluxInert atmosphere;
参考文献
Zhou, Ming; Dong, Dejun; Zhu, Baolin; Geng, Huiling; Wang, Yan; Zhang, Xumu
Organic Letters, 2013 , vol. 15, # 21 p. 5524 - 5527