4,4’-(1,10-癸二氧基)二苯胺合成路线 （共 4 条）
反应条件
palladium 10 on activated carbon; hydrazine hydrate in ethanol; dichloromethane
24 h;
参考文献
Min, Misook; Bang, Gyeong Sook; Lee, Hyoyoung; Yu, Byung-Chan
Chemical Communications, 2010 , vol. 46, # 29 p. 5232 - 5234
反应条件
1: dimethylformamide / 10 h / Heating
2: H2 / 5percent Pd/C / tetrahydrofuran; methanol / 2280 Torr
View Scheme
参考文献
Turner, William R.; Werbel, Leslie M.
Journal of Medicinal Chemistry, 1985 , vol. 28, # 11 p. 1728 - 1740
参考文献
Okahata,Y.; Kunitake,T.
Journal of the American Chemical Society, 1979 , vol. 101, # 18 p. 5231 - 5234
反应条件
1: anhydous K2CO3 / dimethylformamide / 4 h / Heating
2: HCl / ethanol
3: NaHCO3 / H2O / 1 h
View Scheme
参考文献
Griffin; Britt; Hung; Steele
Molecular crystals and liquid crystals, 1983 , vol. 105, # 1-4 p. 305 - 314
