2,2-二甲基-1-苯基-1-丙醇合成路线 （共 26 条）
反应条件
(R)-(+)-N-methylbenzoguanidine; trimethylacetic anhydride in diethyl ether T=20°C; 12 h; Resolution of racemate; optical yield given as percent ee;
参考文献
Nakata, Kenya; Shiina, Isamu
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 20 p. 7092 - 7096
反应条件
(R)-(+)-N-methylbenzoguanidine; trimethylacetic anhydride in diethyl ether T=20°C; 12 h; Resolution of racemate; optical yield given as percent ee;
参考文献
Nakata, Kenya; Shiina, Isamu
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 20 p. 7092 - 7096
反应条件
(R)-(+)-N-methylbenzoguanidine; trimethylacetic anhydride in diethyl ether T=20°C; 12 h; Resolution of racemate; optical yield given as percent ee;
参考文献
Nakata, Kenya; Shiina, Isamu
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 20 p. 7092 - 7096
反应条件
C10H16NO5; potassium carbonate; bis-[(trifluoroacetoxy)iodo]benzene in dichloromethane T=20°C;
参考文献
Hamada, Shohei; Furuta, Takumi; Wada, Yoshiyuki; Kawabata, Takeo
Angewandte Chemie - International Edition, 2013 , vol. 52, # 31 p. 8093 - 8097
Angew. Chem., 2013 , vol. 125, # 31 p. 8251 - 8255,5
反应条件
1: oxidant 2: 3.4 percent Chromat. / Zn(Hg), HCO2H / ethanol / 1 h / Heating View Scheme
参考文献
Synthetic Communications, , vol. 26, # 14 p. 2625 - 2631
反应条件
perchloric acid in 1,4-dioxane T=70°C; 96 h;
参考文献
Laurent,A. et al.
Bulletin de la Societe Chimique de France, 1968 , p. 3307 - 3314
反应条件
C10H16NO5; potassium carbonate; bis-[(trifluoroacetoxy)iodo]benzene in dichloromethane
T=20°C;
参考文献
Hamada, Shohei; Furuta, Takumi; Wada, Yoshiyuki; Kawabata, Takeo
Angewandte Chemie - International Edition, 2013 , vol. 52, # 31 p. 8093 - 8097
Angew. Chem., 2013 , vol. 125, # 31 p. 8251 - 8255,5
反应条件
perchloric acid in 1,4-dioxane
T=70°C; 96 h;
参考文献
Laurent,A. et al.
Bulletin de la Societe Chimique de France, 1968 , p. 3307 - 3314
反应条件
methyltrioxorhenium (VII) in benzene
72 h;
参考文献
Zhu, Zuolin; Espenson, James H.
Journal of Organic Chemistry, 1996 , vol. 61, # 1 p. 324 - 328
反应条件
1: Na2Cr2O7; aqueous sulfuric acid
View Scheme
参考文献
Skell; Hauser
Journal of the American Chemical Society, 1942 , vol. 64, p. 2633
