反应条件
1: 2-hydroxypyrimidine hydrochloride With ammonium sulfate; 1,1,1,3,3,3-hexamethyl-disilazane
4 h; Inert atmosphereReflux;
2: (2R,3R,4R,5S)-4,5-bis(acetyloxy)-2-[(acetyloxy)methyl]tetrahydro-3-furanyl acetate With tin(IV) chloride in dichloromethane
T=20°C; 16 h;
参考文献
Battenberg, Oliver A.; Nodwell, Matthew B.; Sieber, Stephan A.
Journal of Organic Chemistry, 2011 , vol. 76, # 15 p. 6075 - 6087
