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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
喷布洛尔
合成路线
（共 14 条）
90970-95-9
→
反应条件
38363-40-5
喷布洛尔
反应条件
sodium hydroxide in ethanol; water T=73°C; 8 h;
参考文献
Kan, Kazunori; Miyama, Akimasa; Hamaguchi, Shigeki; Ohashi, Takehisa; Watanabe, Kiyoshi
Agricultural and Biological Chemistry, 1985 , vol. 49, # 1 p. 207 - 210
1518-84-9
2-环戊基苯酚
→
反应条件
38363-40-5
喷布洛尔
反应条件
1.1: 91 percent / K2CO3 / acetone / 12 h / 20 °C 2.1: 90 percent / OsO4; K2CO3; H2O / (DHQ)2PHAL; K3Fe(CN)6 / 2-methyl-propan-2-ol / 24 h / 20 °C 3.1: 93 percent / SOCl2; pyridine / 3 h / 0 °C 4.1: 91 percent / RuCl3; NaIO4 / acetonitrile; CCl4; H2O 5.1: tetrahydrofuran / 8 h / Heating 5.2: 72 percent / H2SO4; H2O / diethyl ether / 12 h View Scheme
参考文献
Phukan, Prodeep; Sudalai, Arumugam
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 20 p. 3015 - 3018
75-64-9
叔丁胺
+
254430-81-4
→
反应条件
38363-40-5
喷布洛尔
反应条件
1: in tetrahydrofuran Substitution; ring cleavage; 8 h; Heating; 2: With sulfuric acid; water in diethyl ether Substitution; 12 h;
参考文献
Phukan, Prodeep; Sudalai, Arumugam
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 20 p. 3015 - 3018
96-41-3
环戊醇
→
反应条件
38363-40-5
喷布洛尔
反应条件
1.1: 62 percent / montmorillonite K-10 / 12 h / 120 °C 2.1: 91 percent / K2CO3 / acetone / 12 h / 20 °C 3.1: 90 percent / OsO4; K2CO3; H2O / (DHQ)2PHAL; K3Fe(CN)6 / 2-methyl-propan-2-ol / 24 h / 20 °C 4.1: 93 percent / SOCl2; pyridine / 3 h / 0 °C 5.1: 91 percent / RuCl3; NaIO4 / acetonitrile; CCl4; H2O 6.1: tetrahydrofuran / 8 h / Heating 6.2: 72 percent / H2SO4; H2O / diethyl ether / 12 h View Scheme
参考文献
Phukan, Prodeep; Sudalai, Arumugam
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 20 p. 3015 - 3018
122030-10-8
→
反应条件
38363-40-5
喷布洛尔
反应条件
1.1: 90 percent / OsO4; K2CO3; H2O / (DHQ)2PHAL; K3Fe(CN)6 / 2-methyl-propan-2-ol / 24 h / 20 °C 2.1: 93 percent / SOCl2; pyridine / 3 h / 0 °C 3.1: 91 percent / RuCl3; NaIO4 / acetonitrile; CCl4; H2O 4.1: tetrahydrofuran / 8 h / Heating 4.2: 72 percent / H2SO4; H2O / diethyl ether / 12 h View Scheme
参考文献
Phukan, Prodeep; Sudalai, Arumugam
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 20 p. 3015 - 3018
108-95-2
苯酚
→
反应条件
38363-40-5
喷布洛尔
反应条件
1.1: 62 percent / montmorillonite K-10 / 12 h / 120 °C 2.1: 91 percent / K2CO3 / acetone / 12 h / 20 °C 3.1: 90 percent / OsO4; K2CO3; H2O / (DHQ)2PHAL; K3Fe(CN)6 / 2-methyl-propan-2-ol / 24 h / 20 °C 4.1: 93 percent / SOCl2; pyridine / 3 h / 0 °C 5.1: 91 percent / RuCl3; NaIO4 / acetonitrile; CCl4; H2O 6.1: tetrahydrofuran / 8 h / Heating 6.2: 72 percent / H2SO4; H2O / diethyl ether / 12 h View Scheme
参考文献
Phukan, Prodeep; Sudalai, Arumugam
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 20 p. 3015 - 3018
154531-76-7
+
75-64-9
叔丁胺
→
反应条件
38363-40-5
喷布洛尔
反应条件
water in N,N-dimethyl-formamide 4.5 h; Heating; Yield given;
参考文献
Klunder, Janice M.; Onami, Tetsuo; Sharpless, K. Barry
Journal of Organic Chemistry, 1989 , vol. 54, # 6 p. 1295 - 1304
38363-22-3
→
反应条件
38363-40-5
喷布洛尔
反应条件
2: t-BuOK / tetrahydrofuran / 1 h / 0 °C 3: tetrahydrofuran; ethanol / 12 h / Heating View Scheme
参考文献
Ader, Ulrich; Schneider, Manfred P.
Tetrahedron: Asymmetry, 1992 , vol. 3, # 4 p. 521 - 524
142037-07-8
→
反应条件
38363-40-5
喷布洛尔
反应条件
1: t-BuOK / tetrahydrofuran / 1 h / 0 °C 2: tetrahydrofuran; ethanol / 12 h / Heating View Scheme
参考文献
Ader, Ulrich; Schneider, Manfred P.
Tetrahedron: Asymmetry, 1992 , vol. 3, # 4 p. 521 - 524
254430-79-0
→
反应条件
38363-40-5
喷布洛尔
反应条件
1.1: 93 percent / SOCl2; pyridine / 3 h / 0 °C 2.1: 91 percent / RuCl3; NaIO4 / acetonitrile; CCl4; H2O 3.1: tetrahydrofuran / 8 h / Heating 3.2: 72 percent / H2SO4; H2O / diethyl ether / 12 h View Scheme
参考文献
Phukan, Prodeep; Sudalai, Arumugam
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 20 p. 3015 - 3018
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