3-硝基-4-二甲基氨基偶氮苯合成路线 (共 9 条)
反应条件
1: 2,4-di-Nitrobenzene With potassium borohydride in methanol; dimethyl sulfoxide T=0 - 3°C; Reduction; 0.666667 h; 2: 4-(N,N-dimethylaminophenyl)diazonium tetrafluoroborate in methanol; dimethyl sulfoxide Substitution; 0.5 h;
参考文献
Atroshchenko; Blokhina; Shakhkel'dyan; Grudtsyn; Gitis; Borbulevich; Blokhin; Kaminskii; Shishkin; Andrianov
Russian Journal of Organic Chemistry, 2000 , vol. 36, # 5 p. 684 - 692
反应条件
4-laurylbenzenesulfonic acid sodium salt in chloroform; water T=25°C; 2 h;
参考文献
Chirakadze; Elizbarashvili; Baidoshvili
Russian Journal of Organic Chemistry, 2000 , vol. 36, # 11 p. 1642 - 1645
反应条件
sulfuric acid; water; sodium nitrite T=27°C;
参考文献
Staedel; Bauer
Chemische Berichte, 1886 , vol. 19, p. 1954
参考文献
Meldola
Journal of the Chemical Society, 1884 , vol. 45, p. 116
反应条件
sulfuric acid; nitric acid unter starker Kuehlung;
参考文献
Noelting
Chemische Berichte, 1887 , vol. 20, p. 2997
参考文献
Staedel; Bauer
Chemische Berichte, 1886 , vol. 19, p. 1954
参考文献
Staedel; Bauer
Chemische Berichte, 1886 , vol. 19, p. 1954
参考文献
Staedel; Bauer
Chemische Berichte, 1886 , vol. 19, p. 1954
参考文献
Staedel; Bauer
Chemische Berichte, 1886 , vol. 19, p. 1954