1-(2-乙炔基苯基)甲胺合成路线 （共 3 条）
反应条件
lithium aluminium tetrahydride in diethyl ether
T=-10 - 20°C; 2 h; Inert atmosphere;
参考文献
Varela-Fernandez, Alejandro; Varela, Jesus A.; Saa, Carlos
Synthesis (Germany), 2012 , vol. 44, # 21 art. no. SS-2012-Z0414-PSP, p. 3285 - 3295
反应条件
1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 20 °C / Inert atmosphere
2: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C / Inert atmosphere
3: lithium aluminium tetrahydride / diethyl ether / Inert atmosphere
View Scheme
参考文献
Varela-Fernandez, Alejandro; Varela, Jesus A.; Saa, Carlos
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 11-12 p. 1933 - 1937
反应条件
1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C / Inert atmosphere
2: lithium aluminium tetrahydride / diethyl ether / Inert atmosphere
View Scheme
参考文献
Varela-Fernandez, Alejandro; Varela, Jesus A.; Saa, Carlos
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 11-12 p. 1933 - 1937
