3-(2-脱氧-beta-D-赤式-呋喃戊糖基)-6-甲基呋喃并[2,3-d]嘧啶-2(3H)-酮合成路线 （共 4 条）
反应条件
copper(l) iodide; triethylamine; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide
T=55 - 60°C; 18 h;
参考文献
Loakes, David; Brown, Daniel M.; Salisbury, Stephen A.; McDougall, Mark G.; Neagu, Constantin; Nampalli, Satyam; Kumar, Shiv
Helvetica Chimica Acta, 2003 , vol. 86, # 4 p. 1193 - 1204
反应条件
copper(l) iodide; triethylamine in methanol
Robins and Barr method; 4 h; Heating;
参考文献
Berry, David A.; Jung, Kee-Yong; Wise, Dean S.; Sercel, Anthony D.; Pearson, William H.; Mackie, Hugh; Randolph, John B.; Somers, Robert L.
Tetrahedron Letters, 2004 , vol. 45, # 11 p. 2457 - 2461
反应条件
1: 65 percent / NEt3; CuI / Pd(PPh3)4 / dimethylformamide
2: 95 percent / NEt3; CuI / methanol / 4 h / Heating
View Scheme
参考文献
Berry, David A.; Jung, Kee-Yong; Wise, Dean S.; Sercel, Anthony D.; Pearson, William H.; Mackie, Hugh; Randolph, John B.; Somers, Robert L.
Tetrahedron Letters, 2004 , vol. 45, # 11 p. 2457 - 2461
反应条件
1: 87 percent / pyridine / CH2Cl2
2: 49 percent / NH3 / methanol; tetrahydrofuran / 22 h / 50 °C
View Scheme
参考文献
Berry, David A.; Jung, Kee-Yong; Wise, Dean S.; Sercel, Anthony D.; Pearson, William H.; Mackie, Hugh; Randolph, John B.; Somers, Robert L.
Tetrahedron Letters, 2004 , vol. 45, # 11 p. 2457 - 2461
