1.1: BuLi / hexane; tetrahydrofuran / 2 h / -78 - 0 °C
1.2: 80 percent / tetrahydrofuran; hexane / -78 - 20 °C
2.1: 15 percent / O2; NaOAc*3H2O / (neocuproine)Pd(OAc)2 / H2O; dimethylsulfoxide / 4 h / 80 °C / 22502.3 Torr
View Scheme
参考文献
Ten Brink, Gerd-Jan; Arends, Isabel W. C. E.; Hoogenraad, Marcel; Verspui, Goeran; Sheldon, Roger A.
Advanced Synthesis and Catalysis, 2003 , vol. 345, # 12 p. 1341 - 1352
1.1: BuLi / hexane; tetrahydrofuran / 2 h / -78 - 0 °C
1.2: 80 percent / tetrahydrofuran; hexane / -78 - 20 °C
2.1: 15 percent / O2; NaOAc*3H2O / (neocuproine)Pd(OAc)2 / H2O; dimethylsulfoxide / 4 h / 80 °C / 22502.3 Torr
View Scheme
参考文献
Ten Brink, Gerd-Jan; Arends, Isabel W. C. E.; Hoogenraad, Marcel; Verspui, Goeran; Sheldon, Roger A.
Advanced Synthesis and Catalysis, 2003 , vol. 345, # 12 p. 1341 - 1352