2-硝基-Alpha,Alpha,Alpha-三氟甲苯合成路线 （共 51 条）
反应条件
in N,N,N',N',N'',N''-hexamethylphosphoric triamide; N,N-dimethyl-formamide T=60 - 70°C; 6 h;
参考文献
Wiemers, Denise M.; Burton, Donald J.
Journal of the American Chemical Society, 1986 , vol. 108, # 4 p. 832 - 834
反应条件
triethylamine tris(hydrogen fluoride) in N,N-dimethyl-formamide T=23 - 50°C; 18 h; Inert atmosphere;
参考文献
Lishchynskyi, Anton; Novikov, Maxim A.; Martin, Eddy; Escudero-Adan, Eduardo C.; Novak, Petr; Grushin, Vladimir V.
Journal of Organic Chemistry, 2013 , vol. 78, # 22 p. 11126 - 11146
反应条件
sulfuric acid; hypophosphorous ether; sodium nitrite
参考文献
Fukui et al.
Nippon Kagaku Zasshi, 1958 , vol. 79, p. 889,892
Chem.Abstr., 1960 , p. 4430
反应条件
2: NaOH-solution / Verseifung View Scheme
参考文献
Pouterman; Girardet
Helvetica Chimica Acta, 1947 , vol. 30, p. 107,110
反应条件
antimony(V) pentachloride; nitryl chloride in dichloromethane T=20°C; 0.25 h; Yield given. Yields of byproduct given;
参考文献
Laali; Gettwert
Journal of Organic Chemistry, 2001 , vol. 66, # 1 p. 35 - 40
反应条件
isobutyramide; copper T=100°C; 16 h;
参考文献
Clark, James H.; Denness, James E.; McClinton, Martin A.; Wynd, Andrew J.
Journal of Fluorine Chemistry, 1990 , vol. 50, # 3 p. 411 - 426
反应条件
copper(l) iodide; 1,10-phenanthroline; cesium fluoride in diethylene glycol dimethyl ether T=80°C; 24 h; Inert atmosphere;
参考文献
Kondo, Hideaki; Oishi, Masahiro; Fujikawa, Kenichi; Amii, Hideki
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 8 p. 1247 - 1252
反应条件
ethanol; sulfuric acid T=0 - 10°C; Erwaermen der Reaktionsloesung mit Kupferbronze;
参考文献
Jones
Journal of the American Chemical Society, 1947 , vol. 69, p. 2352
反应条件
isobutyramide; copper T=100°C; 8 h;
参考文献
Clark, James H.; Denness, James E.; McClinton, Martin A.; Wynd, Andrew J.
Journal of Fluorine Chemistry, 1990 , vol. 50, # 3 p. 411 - 426
反应条件
iron (III) acetylacetonate; oxygen; nitrogen(IV) oxide; ozone in dichloromethane T=0°C; 5 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Aridoss, Gopalakrishnan; Laali, Kenneth K.
Journal of Organic Chemistry, 2011 , vol. 76, # 19 p. 8088 - 8094
