2-硝基-Alpha,Alpha,Alpha-三氟甲苯合成路线 （共 51 条）
反应条件
isobutyramide; copper T=100°C; 4 h;
参考文献
Clark, James H.; Denness, James E.; McClinton, Martin A.; Wynd, Andrew J.
Journal of Fluorine Chemistry, 1990 , vol. 50, # 3 p. 411 - 426
反应条件
potassium fluoride in N,N-dimethyl acetamide T=50°C; Title compound not separated from byproducts;
参考文献
Adams, Dave J.; Clark, James H.; Hansen, Liv B.; Sanders, Victoria C.; Tavener, Stewart J.
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 18 p. 3081 - 3085
反应条件
potassium fluoride in N,N-dimethyl acetamide T=50°C;
参考文献
Adams, Dave J.; Clark, James H.; Hansen, Liv B.; Sanders, Victoria C.; Tavener, Stewart J.
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 18 p. 3081 - 3085
反应条件
pyridine T=110 - 115°C; 24 h;
参考文献
Yazdanbakhsh, Mohammad R.; Mahmoodi, Nosrat O.; Dabiry, Shahram
Mendeleev Communications, 2006 , # 3 p. 192 - 194
反应条件
anhydrous potassium trifluoroacetate in water; acetonitrile T=25°C; electrochemical reaction, total electricity of 0.082 F, the anode was platinum gauze, the cathode was made of GC-2000 glassy carbon. The current density was 33 mA cm-2.; Yield given. Yields of byproduct given;
参考文献
Grinberg; Lundgren; Sterlin; Mysov
Russian Chemical Bulletin, 1997 , vol. 46, # 6 p. 1131 - 1135
反应条件
1: aq. H2SO4 2: (i) H2SO4, EtNO2, EtOH, (ii) Cu View Scheme
参考文献
Forbes,E.J. et al.
Tetrahedron, 1960 , vol. 8, p. 67 - 72
反应条件
[2,2']bipyridinyl; tetrabutylammomium bromide 1.) DMF, -15 deg C, 3.5 h, electrolysis, 2.) DMF, 80 deg C, 5 h; Yield given. Multistep reaction;
参考文献
Paratian, J. M.; Labbe, E.; Sibille, S.; Perichon, J.
Journal of Organometallic Chemistry, 1995 , vol. 489, # 1-2 p. 137 - 144
反应条件
N,N'-dimethyl-N,N'-propyleneurea; potassium fluoride; copper(l) iodide heating;
参考文献
MacNeil, James G.; Burton, Donald J.
Journal of Fluorine Chemistry, 1991 , vol. 55, # 2 p. 225 - 228
反应条件
1: NaOH-solution / Verseifung View Scheme
参考文献
Rouche
Bulletin de la Classe des Sciences, Academie Royale de Belgique, 1927 , vol. <5> 13, p. 349
Chem. Zentralbl., 1927 , vol. 98, # II p. 1817
参考文献
Pouterman; Girardet
Helvetica Chimica Acta, 1947 , vol. 30, p. 107,110
