2-硝基-Alpha,Alpha,Alpha-三氟甲苯合成路线 （共 51 条）
参考文献
Rouche
Bulletin de la Classe des Sciences, Academie Royale de Belgique, 1927 , vol. <5> 13, p. 349
Chem. Zentralbl., 1927 , vol. 98, # II p. 1817
参考文献
Pouterman; Girardet
Helvetica Chimica Acta, 1947 , vol. 30, p. 107,110
反应条件
(i) H2, Raney-Ni, EtOH, (ii) (acetylation); Multistep reaction;
参考文献
Jones
Journal of the American Chemical Society, 1947 , vol. 69, p. 2352
反应条件
bismuth; hydrogen fluoride in dichloromethane Yields of byproduct given;
参考文献
Journal of Fluorine Chemistry, , vol. 74, # 2 p. 251 - 254
反应条件
tert.-butylhydroperoxide; potassium tert-butylate in ammonia T=-33°C;
参考文献
Makosza, Mieczyslaw; Sienkiewicz, Krzysztof
Journal of Organic Chemistry, 1998 , vol. 63, # 13 p. 4199 - 4208
反应条件
1: lead; sodium acetate; aqueous ethanol / bei der elektrochemischen Reduktion 2: sodium-amalgam; ethanol 3: H2SO4 View Scheme
参考文献
Cartwright; Tatlow
Journal of the Chemical Society, 1953 , p. 1994,1996
反应条件
2,4,6-trichlorosulfenamide; potassium tert-butylate in N,N-dimethyl-formamide T=20°C; 0.333333 h;
参考文献
Makosza, Mieczyslaw; Bialecki, Maciej
Journal of Organic Chemistry, 1998 , vol. 63, # 15 p. 4878 - 4888
反应条件
potassium tert-butylate; N,N-tetramethylene-thiocarbamoyl-sulphenamide in N,N-dimethyl-formamide T=20°C; 0.333333 h;
参考文献
Makosza, Mieczyslaw; Bialecki, Maciej
Journal of Organic Chemistry, 1998 , vol. 63, # 15 p. 4878 - 4888
反应条件
2,4,6-trichlorosulfenamide; potassium tert-butylate in N,N-dimethyl-formamide T=20°C; 0.333333 h;
参考文献
Makosza, Mieczyslaw; Bialecki, Maciej
Journal of Organic Chemistry, 1998 , vol. 63, # 15 p. 4878 - 4888
反应条件
1: palladium / Hydrogenation 2: Diazotization.Behandlung der Diazoniumsalz-Loesung mit KI View Scheme
参考文献
Jones
Journal of the American Chemical Society, 1947 , vol. 69, p. 2352
