1,2-二甲氧基-4-(甲氧甲基)苯合成路线 （共 17 条）
反应条件
ammonium cerium(IV) nitrate; water in acetonitrile 2 h; Ambient temperature;
参考文献
Badea; Cotelle; Catteau
Synthetic Communications, 1994 , vol. 24, # 14 p. 2011 - 2016
反应条件
laccase; oxygen; benzotriazol-1-ol in various solvent(s) T=20°C; 24 h; Product distribution; Further Variations:Reagents;
参考文献
Organic and Biomolecular Chemistry, , vol. 1, # 1 p. 191 - 197
反应条件
hydrogenchloride; water in tetrahydrofuran T=70°C; 1.5 h;
参考文献
Roe, Caroline; Sandoe, Elizabeth J.; Richard Stephenson
Tetrahedron Letters, 2010 , vol. 51, # 4 p. 591 - 595
反应条件
laccase; oxygen; benzotriazol-1-ol in various solvent(s) T=20°C; 24 h; Product distribution; Further Variations:Reagents;
参考文献
Organic and Biomolecular Chemistry, , vol. 1, # 1 p. 191 - 197
反应条件
sodium hydride in tetrahydrofuran
T=0 - 20°C; 3 h;
参考文献
THE GOVERNMENT OF THE UNITED STATES, AS REPRESENTED BY THE SECRETARY OF HEALTH AND HUMAN SERVICES, NATIONAL INSTITUTES OF HEALTH, OFFICE OF TECHNOLOGY TRANSFER
Patent: WO2009/26248 A2, 2009 ;
Location in patent: Page/Page column 33; 34 ;
反应条件
1: NaBH4 / methanol
2: NaH / dimethylsulfoxide
View Scheme
参考文献
Pincock, J. A.; Wedge, P. J.
Journal of Organic Chemistry, 1994 , vol. 59, # 19 p. 5587 - 5595
反应条件
1: sodium borohydride / ethanol / 1 h
2: 1) sodium hydride / 1) THF, room temp., 1 h; 2) room temp.
3: 1) LDA / 1) THF, -78 deg C, 10 min; 2) THF, -40 deg C, then 2 h to room temp.
View Scheme
参考文献
Khanapure, Subhash P.; Biehl, Edward R.
Journal of Organic Chemistry, 1990 , vol. 55, # 5 p. 1471 - 1475
反应条件
1: pyridine / benzene / Ambient temperature
2: 43 percent Chromat. / methanol / Irradiation
View Scheme
参考文献
Pincock, J. A.; Wedge, P. J.
Journal of Organic Chemistry, 1994 , vol. 59, # 19 p. 5587 - 5595
参考文献
Sharp,D.B.; Patrick,T.M.
Journal of Organic Chemistry, 1961 , vol. 26, p. 1389 - 1394
反应条件
1: 1) sodium hydride / 1) THF, room temp., 1 h; 2) room temp.
2: 1) LDA / 1) THF, -78 deg C, 10 min; 2) THF, -40 deg C, then 2 h to room temp.
View Scheme
参考文献
Khanapure, Subhash P.; Biehl, Edward R.
Journal of Organic Chemistry, 1990 , vol. 55, # 5 p. 1471 - 1475
