3,4,5-三甲氧基苄醇合成路线 （共 102 条）
反应条件
sodium amalgam; ethanol; water Reaktion ueber mehrere Stufen;
参考文献
Heffter; Capellmann
Chemische Berichte, 1905 , vol. 38, p. 3636
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Marx
Justus Liebigs Annalen der Chemie, 1891 , vol. 263, p. 255
反应条件
1: tetrachloroethane; SnCl2; etheric HCl / 0 °C / Erhitzen des Reaktionsprodukts mit wss.HCl und Essigsaeure 2: ethanol; platinum / Hydrogenation View Scheme
参考文献
Cook et al.
Journal of the Chemical Society, 1944 , p. 322,324
反应条件
1: LiAlH4 2: K2CO3 View Scheme
参考文献
Ahluwalia,V.K.; Kumar,D.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1977 , vol. 15B, p. 18 - 20
反应条件
ethanol; sodium ethanolate
参考文献
Cook et al.
Journal of the Chemical Society, 1944 , p. 322,324
参考文献
Ahluwalia,V.K.; Kumar,D.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1977 , vol. 15B, p. 18 - 20
反应条件
Co(III)W in water; acetic acid 1 h; Ambient temperature; Product distribution;
参考文献
Baciocchi, Enrico; Lanzalunga, Osvaldo; Pirozzi, Bruno
Tetrahedron, 1997 , vol. 53, # 36 p. 12287 - 12298
参考文献
Graebe; Suter
Justus Liebigs Annalen der Chemie, 1905 , vol. 340, p. 230
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Marx
Justus Liebigs Annalen der Chemie, 1891 , vol. 263, p. 255
反应条件
1: SOCl2 / CHCl3 / 1 h / 20 °C 2: 17.49 g / 1,2-dichloro-benzene / 0.08 h / Heating View Scheme
参考文献
Rosowsky, Andre; Papoulis, Andrew T.; Forsch, Ronald A.; Queener, Sherry F.
Journal of Medicinal Chemistry, 1999 , vol. 42, # 6 p. 1007 - 1017
反应条件
1: thionyl chloride / dichloromethane 2: dimethyl sulfoxide 3: potassium hydroxide; water / ethanol / 15 h / |Reflux 4: lithium aluminium tetrahydride / tetrahydrofuran / 3.5 h / 20 °C / |Reflux View Scheme
参考文献
Zheng, Cheng; Guo, Yibing; Meng, Ying; Dou, Sufeng; Shao, Jian; Yang, Yumin
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2013 , vol. 52, # 5 p. 654 - 664
反应条件
thionyl chloride in dichloromethane T=0 - 23°C;
参考文献
Percec, Virgil; Won, Betty C.; Peterca, Mihai; Heiney, Paul A.
Journal of the American Chemical Society, 2007 , vol. 129, # 36 p. 11265 - 11278
