2,2',3,3',6,6'-六氯联苯合成路线 （共 19 条）
反应条件
copper T=230°C; 48 h;
参考文献
Waller, Stephen C.; Mash, Eugene A.
Organic Preparations and Procedures International, 1997 , vol. 29, # 6 p. 679 - 685
反应条件
copper T=230°C; 552 h;
参考文献
Waller, Stephen C.; He, You Ai; Harlow, Greg R.; He, You Qun; Mash, Eugene A.; Halpert, James R.
Chemical Research in Toxicology, 1999 , vol. 12, # 8 p. 690 - 699
反应条件
copper T=230°C; 168 h;
参考文献
Waller, Stephen C.; He, You Ai; Harlow, Greg R.; He, You Qun; Mash, Eugene A.; Halpert, James R.
Chemical Research in Toxicology, 1999 , vol. 12, # 8 p. 690 - 699
反应条件
1: 44 percent / HNO3; H2SO4 / 72 h / 20 °C 2: 92 percent / Na2S2O4 / aq. ethanol / 4 h / Heating 3: 31 percent / Cu / 552 h / 230 °C View Scheme
参考文献
Waller, Stephen C.; He, You Ai; Harlow, Greg R.; He, You Qun; Mash, Eugene A.; Halpert, James R.
Chemical Research in Toxicology, 1999 , vol. 12, # 8 p. 690 - 699
反应条件
1: 36 percent / H2O2; HCl / CHCl3 / 14 h / 20 °C 2: 39 percent / Cu / 168 h / 230 °C View Scheme
参考文献
Waller, Stephen C.; He, You Ai; Harlow, Greg R.; He, You Qun; Mash, Eugene A.; Halpert, James R.
Chemical Research in Toxicology, 1999 , vol. 12, # 8 p. 690 - 699
反应条件
1: 92 percent / Na2S2O4 / aq. ethanol / 4 h / Heating 2: 31 percent / Cu / 552 h / 230 °C View Scheme
参考文献
Waller, Stephen C.; He, You Ai; Harlow, Greg R.; He, You Qun; Mash, Eugene A.; Halpert, James R.
Chemical Research in Toxicology, 1999 , vol. 12, # 8 p. 690 - 699
反应条件
1: 59 percent / Cu / 288 h / 230 °C 2: SO2Cl2, AlCl3 / CH2Cl2 / 1 h / Ambient temperature View Scheme
参考文献
Waller, Stephen C.; Mash, Eugene A.
Organic Preparations and Procedures International, 1997 , vol. 29, # 6 p. 679 - 685
反应条件
1: 1.) NaNO2, aq. H2SO4, 2.) KI / 1.) 0-5 deg C, 10 min, 2.) 0 deg C, 15 min; r.t., 1 h 2: 59 percent / Cu / 288 h / 230 °C 3: SO2Cl2, AlCl3 / CH2Cl2 / 1 h / Ambient temperature View Scheme
参考文献
Waller, Stephen C.; Mash, Eugene A.
Organic Preparations and Procedures International, 1997 , vol. 29, # 6 p. 679 - 685
反应条件
aluminium trichloride; sulfuryl dichloride in dichloromethane 1 h; Ambient temperature; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Waller, Stephen C.; Mash, Eugene A.
Organic Preparations and Procedures International, 1997 , vol. 29, # 6 p. 679 - 685
反应条件
1: 31 percent / Cu / 552 h / 230 °C View Scheme
参考文献
Waller, Stephen C.; He, You Ai; Harlow, Greg R.; He, You Qun; Mash, Eugene A.; Halpert, James R.
Chemical Research in Toxicology, 1999 , vol. 12, # 8 p. 690 - 699
