N-(4-溴苯基)-3-氧丁酰胺合成路线 （共 18 条）
反应条件
1: 25.6 percent / conc. H2SO4 / 120 °C 2: 97 percent / POCl3 / Heating View Scheme
参考文献
Wlodarczyk, Nicolas; Simenel, Catherine; Delepierre, Muriel; Barale, Jean-Christophe; Janin, Yves L.
Synthesis, 2011 , # 6 art. no. T51110SS, p. 934 - 942
反应条件
in cyclohexane T=25°C; Equilibrium constant;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 50, # 2 p. 365 - 374
参考文献
Piala, Alexander; Mayi, Diyar; Handy, Scott T.
Tetrahedron, 2011 , vol. 67, # 23 p. 4147 - 4154
反应条件
in cyclohexane T=25°C; Equilibrium constant;
参考文献
Knizek, Jiri; Lejdar, Erhard; Vetesnik, Pavel
Collection of Czechoslovak Chemical Communications, 1985 , vol. 50, # 2 p. 365 - 374
反应条件
1.1: sulfuric acid / 1.5 h / 120 °C 2.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h 2.2: 1 h View Scheme
参考文献
Piala, Alexander; Mayi, Diyar; Handy, Scott T.
Tetrahedron, 2011 , vol. 67, # 23 p. 4147 - 4154
反应条件
acetic acid; sodium nitrite in water
T=5 - 20°C;
参考文献
Mloston, Grzegorz; Jasinski, Marcin
Collection of Czechoslovak Chemical Communications, 2010 , vol. 75, # 8 p. 871 - 885
反应条件
1: 25.6 percent / conc. H2SO4 / 120 °C
2: 97 percent / POCl3 / Heating
3: 74 percent / ethanol / Heating
View Scheme
参考文献
Davis, Steven E.; Rauckman, Barbara S.; Chan, Joseph H.; Roth, Barbara
Journal of Medicinal Chemistry, 1989 , vol. 32, # 8 p. 1936 - 1942
反应条件
1: 25.6 percent / conc. H2SO4 / 120 °C
2: 97 percent / POCl3 / Heating
3: 74 percent / ethanol / Heating
4: 1) n-BuLi / 1) THF, hexane, -78 deg C, 5 min, 2) to -20 deg C
View Scheme
参考文献
Davis, Steven E.; Rauckman, Barbara S.; Chan, Joseph H.; Roth, Barbara
Journal of Medicinal Chemistry, 1989 , vol. 32, # 8 p. 1936 - 1942
