ALPHA-氯-4-甲氧基苯甲醛肟合成路线 (共 51 条)
反应条件
triethylamine in diethyl ether 48 h; Ambient temperature;
参考文献
Albini, Franca Marinone; Franco, Rita De; Bandiera, Tiziano; Caramella, Pierluigi; Corsaro, Antonino; Perrini, Giancarlo
Journal of Heterocyclic Chemistry, 1989 , vol. 26, p. 757 - 761
反应条件
triethylamine in ethyl acetate
参考文献
Weidner-Wells, Michele A.; Henninger, Todd C.; Fraga-Spano, Stephanie A.; Boggs, Christine M.; Matheis, Michele; Ritchie, David M.; Argentieri, Dennis C.; Wachter, Michael P.; Hlasta, Dennis J.
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 16 p. 4307 - 4311
反应条件
sodium hydrogencarbonate in water; isopropyl alcohol T=20°C; 4 h; regioselective reaction;
参考文献
Journal of the Iranian Chemical Society, , vol. 11, # 2 p. 361 - 367
反应条件
triethylamine in diethyl ether T=-15°C;
参考文献
Cristina, D.; Amici, M. De; Micheli, C. De; Gandolfi, R.
Tetrahedron, 1981 , vol. 37, p. 1349 - 1357
反应条件
1: 91 percent / Et3N / diethyl ether / Ambient temperature 2: 1) (COCl)2, DMSO, 3) Et3N 3: 60 percent / H2, 42percent aq. HBF3 / Raney Ni / ethanol / 16 h / 760 Torr / Ambient temperature View Scheme
参考文献
Kanemasa Asai; Tanaka
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 2 p. 375 - 380
反应条件
1: 5 wt Cu/Fe / 3 h / 100 °C 2: hydrazine hydrate / N,N-dimethyl-formamide / 2 h / 100 °C View Scheme
参考文献
Kovacs, Szabolcs; Novak, Zoltan
Tetrahedron, 2013 , vol. 69, # 43 p. 8987 - 8993
反应条件
triethylamine in acetonitrile T=80°C; 4 h;
参考文献
Prasanna, Pitchaimani; Kumar, Sundaravel Vivek; Gunasekaran, Pethaiah; Perumal, Subbu
Tetrahedron Letters, 2013 , vol. 54, # 29 p. 3740 - 3743
反应条件
triethylamine; thiourea in tetrahydrofuran Ambient temperature;
参考文献
Kim, Jae Nyoung; Ryu, Eung K.
Tetrahedron Letters, 1993 , vol. 34, # 51 p. 8283 - 8284
反应条件
1: With triethylamine in tetrahydrofuran T=20°C; 0.5 h; PS-DVB resin; 2: in dichloromethane T=100°C; 0.333333 h; PS-DVB resin;
参考文献
Burkett, Brendan A.; Fu, Pincheng; Hewitt, Russell J.; Ng, Su Ling; Toh, Joel D. W.
European Journal of Organic Chemistry, 2014 , vol. 2014, # 5 p. 1053 - 1058
反应条件
triethylamine in tetrahydrofuran Ambient temperature; Yield given;
参考文献
Kim, Jae Nyoung; Jung, Keum Shin; Lee, Hong Jung; Son, Ji Suk
Tetrahedron Letters, 1997 , vol. 38, # 9 p. 1597 - 1598