sodium tetrahydroborate in dimethyl sulfoxide; benzene Irradiation (UV/VIS); mixt. of substrate and mercurial is irradiated in nitrogen-purged solvent in Pyrex tube with 275-W sunlamp for 2 h; mixt. is worked up with NaBH4, (1)H-NMR;
in dimethyl sulfoxide; benzene Irradiation (UV/VIS); mixt. of substrate and mercurial is irradiated in nitrogen-purged solvent in Pyrex tube with 275-W sunlamp for 2 h; mixt. is poured into water, extd., extract is washed twice with aq. sodium thiosulfate, dried over anhyd. Na2SO4, concd.; (1)H-NMR;
参考文献
Russell, Glen A.; Ngoviwatchai, Preecha; Tashtoush, Hasan I.
Organometallics, 1988 , vol. 7, p. 696 - 702
potassium iodide in dimethyl sulfoxide T=35 - 40°C; 0.5 h; Irradiationalso in the presence of PTSA; various time and molar equiv.; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 60, # 17 p. 5390 - 5395
