紫外线吸收剂UV-320合成路线 （共 13 条）
反应条件
sodium hydroxide in tetrahydrofuran; water electrolysis, Pt cathode and anode;
参考文献
Kim, Byeong Hyo; Kim, Sun Kyong; Lee, Yoon Seok; Jun, Young Moo; Baik, Woonphil; Lee, Byung Min
Tetrahedron Letters, 1997 , vol. 38, # 48 p. 8303 - 8306
反应条件
sodium hydroxide; thiourea dioxide in ethanol T=85 - 90°C; 1 h;
参考文献
Baik, Woonphil; Park, Tae Hong; Kim, Byeong Hyo; Jun, Young Moo
Journal of Organic Chemistry, 1995 , vol. 60, p. 5683 - 5685
反应条件
sulfuric acid; sodium; sodium hydrogensulfite in water; isopropyl alcohol
参考文献
Ciba-Geigy Corporation
Patent: US4642350 A1, 1987 ;
反应条件
sodium hydroxide in cyclohexanol
参考文献
Ciba-Geigy Corporation
Patent: US4642350 A1, 1987 ;
反应条件
sodium hydroxide; hydroxylamine hydrochloride in ethanol 0.5 h; Heating;
参考文献
Baik, Woonphil; Yoo, Chang Hyun; Koo, Sangho; Kim, Hern; Hwang, Yong Hyun; Kim, Byeong Hyo; Lee, Seok Woo
Heterocycles, 1999 , vol. 51, # 8 p. 1779 - 1783
反应条件
sodium hydroxide; zinc in ethanol 5 h; Heating;
参考文献
Rosevear, Judi; Wilshire, John F. K.
Australian Journal of Chemistry, 1982 , vol. 35, # 10 p. 2089 - 2093
反应条件
1: 2.) 1N HCl, sodium lauryl sulfate / 1.) diazotation, 2.) 45 deg C, 6 h 2: 91 percent / glucose, 2N NaOH / ethanol / 1 h / Heating 3: 79 percent / Zn, 2N NaOH / ethanol / 1 h / Ambient temperature View Scheme
参考文献
Rosevear, Judi; Wilshire, John F. K.
Australian Journal of Chemistry, 1982 , vol. 35, # 10 p. 2089 - 2093
反应条件
1: 2.) 1N HCl, sodium lauryl sulfate / 1.) diazotation, 2.) 45 deg C, 6 h 2: 91 percent / glucose, 2N NaOH / ethanol / 1 h / Heating 3: 79 percent / Zn, 2N NaOH / ethanol / 1 h / Ambient temperature View Scheme
参考文献
Rosevear, Judi; Wilshire, John F. K.
Australian Journal of Chemistry, 1982 , vol. 35, # 10 p. 2089 - 2093
反应条件
1: 84 percent / glucose, 2N NaOH / ethanol / 1 h / Heating 2: 88 percent / Zn, 2N NaOH / ethanol / 1 h / Ambient temperature 3: 73 percent / Zn, 2N NaOH / ethanol / 5 h / Heating View Scheme
参考文献
Rosevear, Judi; Wilshire, John F. K.
Australian Journal of Chemistry, 1982 , vol. 35, # 10 p. 2089 - 2093
反应条件
1: 88 percent / Zn, 2N NaOH / ethanol / 1 h / Ambient temperature 2: 73 percent / Zn, 2N NaOH / ethanol / 5 h / Heating View Scheme
参考文献
Rosevear, Judi; Wilshire, John F. K.
Australian Journal of Chemistry, 1982 , vol. 35, # 10 p. 2089 - 2093
