紫外线吸收剂UV-320合成路线 (共 13 条)
反应条件
1: 2.) 1N HCl, sodium lauryl sulfate / 1.) diazotation, 2.) 45 deg C, 6 h 2: 84 percent / glucose, 2N NaOH / ethanol / 1 h / Heating 3: 88 percent / Zn, 2N NaOH / ethanol / 1 h / Ambient temperature 4: 73 percent / Zn, 2N NaOH / ethanol / 5 h / Heating View Scheme
参考文献
Rosevear, Judi; Wilshire, John F. K.
Australian Journal of Chemistry, 1982 , vol. 35, # 10 p. 2089 - 2093
反应条件
2-Bromo-2-nitropropane; zinc in methanol; dichloromethane 4 h; Ambient temperature;
参考文献
Kim, Byeong Hyo; Lee, Yoon Seok; Kwon, Woong; Jin, Youngoo; Tak, Jung Ae; Jun, Young Moo; Baik, Woonphil; Lee, Byung Min
Heterocycles, 1998 , vol. 48, # 12 p. 2581 - 2592
反应条件
aluminium trichloride; nitromethane in toluene 7 h; Heating;
参考文献
Australian Journal of Chemistry, , vol. 38, # 8 p. 1163 - 1176