4-甲氧基-2-硝基苯腈合成路线 (共 24 条)
反应条件
1: iron; aq.-ethanolic hydrochloric acid 2: aqueous acetic acid 3: aqueous HCl 4: POCl3; PCl5 View Scheme
参考文献
Journal of the Chemical Society, , p. 1759,1765
反应条件
1: With diisobutylaluminium hydride in diethyl ether; toluene T=0°C; 0.333333 h; 2: With silica gel in diethyl ether; toluene Further stages.;
参考文献
Gallou-Dagommer, Isabelle; Gastaud, Philippe; RajanBabu
Organic Letters, 2001 , vol. 3, # 13 p. 2053 - 2056
反应条件
1.1: 100 percent / SnCl2; AcOH / 1,2-dimethoxy-ethane; ethanol / 3 h / 65 °C 2.1: NaNO2; HCl / H2O / 0.5 h / 0 °C 2.2: 61 percent / KI / H2O / 0 - 20 °C 3.1: 16 percent / triethylamine; palladium bis(dibenzylideneacetone) / dimethylformamide; H2O / 48 h / 130 °C View Scheme
参考文献
Pletnev, Alexandre A.; Tian, Qingping; Larock, Richard C.
Journal of Organic Chemistry, 2002 , vol. 67, # 26 p. 9276 - 9287
反应条件
borane-THF in tetrahydrofuran
19 h;
参考文献
Johnson, Erik C. B.; Kent, Stephen B. H.
Chemical Communications, 2006 , # 14 p. 1557 - 1559