(1,1-二苯基-1-丙烯-2-基)二叔丁基膦合成路线 (共 2 条)
反应条件
iodine; magnesium; copper chloride in tetrahydrofuran; n-heptane; ethyl acetate
反应条件
1: 2-bromo-1,1-diphenylpropene With iodine; magnesium in tetrahydrofuran 2 h; Heating; 2: chlorodi-tert-butylphosphine With copper(l) iodide in tetrahydrofuran 18 h; Heating; 3: With ammonium hydroxide in ethyl acetate Further stages.;
参考文献
Advanced Synthesis and Catalysis, , vol. 349, # 13 p. 2089 - 2091