2-(羟)-5,6-(亚甲二氧基)-1-茚酮合成路线 （共 3 条）
反应条件
sulfuric acid; hydrogen; palladium on activated charcoal in acetic acid P=2585.7 Torr; 18 h;
参考文献
Nichols, David E.; Brewster, William K.; Johnson, Michael P.; Oberlender, Robert; Riggs, Robert M.
Journal of Medicinal Chemistry, 1990 , vol. 33, # 2 p. 703 - 710
反应条件
p-toluenesulfonyl chloride; sodium hydroxide in water
参考文献
Wu, Meng; Li, Ling; Feng, An-Zheng; Su, Bo; Liang, De-Min; Liu, Yu-Xiu; Wang, Qing-Min
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 7 p. 2539 - 2542
反应条件
1: 78 percent / sodium borohydride / ethanol / 24 h / 23 °C
2: 61 percent / p-toluene-sulfonyl chloride / pyridine / 2.5 h / Ambient temperature
3: 77 percent / molecular sieves / CH2Cl2 / 2 h / Ambient temperature
View Scheme
参考文献
Cushman, Mark; Dikshit, Dinesh K.
Journal of Organic Chemistry, 1980 , vol. 45, # 25 p. 5064 - 5067
