5-甲基-2-硝基苯甲醚合成路线 (共 55 条)
反应条件
1: potassium carbonate / dimethylformamide / 14 h / Ambient temperature 2: 17 percent / potassium carbonate, copper(II) oxide / 16 h / 140 °C View Scheme
参考文献
Carvalho, Christopher F.; Sargent, Melvyn V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 7 p. 1613 - 1620
参考文献
Reissert
Chemische Berichte, 1898 , vol. 31, p. 398
Chem. Zentralbl., 1898 , vol. 69, # I p. 296
反应条件
toluene T=110 - 120°C;
参考文献
Khotinsky; Jacopson-Jacopmann
Chemische Berichte, 1909 , vol. 42, p. 3101
反应条件
1: 26 percent / copper(II) nitrate trihydrate, acetic anhydride / 1.5 h / 30 °C 2: 17 percent / potassium carbonate, copper(II) oxide / 16 h / 140 °C View Scheme
参考文献
Carvalho, Christopher F.; Sargent, Melvyn V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 7 p. 1613 - 1620
反应条件
1: nitric acid View Scheme
参考文献
Schiemann
Chemische Berichte, 1929 , vol. 62, p. 1804
反应条件
in methanol T=30 - 50°C; Rate constant;
参考文献
Patil, Sampatrao D.; Nair, P. Madhavan
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1988 , p. 637 - 640
参考文献
Tschitschibabin
Bulletin de la Societe Chimique de France, 1937 , vol. <5> 4, p. 439
参考文献
Schiemann
Chemische Berichte, 1929 , vol. 62, p. 1804
参考文献
Kenner; Parkin
Journal of the Chemical Society, 1920 , vol. 117, p. 856
反应条件
hydrogen; palladium on activated charcoal in ethanol Reduction; 1 h;
参考文献
Coleman; Guernon; Roland
Organic letters, 2000 , vol. 2, # 3 p. 277 - 280