2-氨基-4氢-色烯-4-酮合成路线 （共 13 条）
反应条件
trichlorophosphate T=80°C; 5 h;
参考文献
Ghosh, Tarun; Sur, Kumar Ranabir; Bandyopadhyay, Chandrakanta
Journal of Chemical Research, 2006 , # 10 p. 651 - 654
反应条件
morpholine; water in N,N-dimethyl-formamide
T=60°C; 2 h;
参考文献
Sosnovskikh, Vyacheslav Ya.; Moshkin, Vladimir S.; Kodess, Mikhail I.
Tetrahedron, 2008 , vol. 64, # 34 p. 7877 - 7889
反应条件
triethylamine in N,N-dimethyl-formamide
7 h; Heating;
参考文献
Ghosh, Tarun; Saha, Satyajit; Bandyopadhyay, Chandrakanta
Synthesis, 2005 , # 11 art. no. T14704SS, p. 1845 - 1849
反应条件
hydrogenchloride in methanol
reflux; 12 h, RT;
参考文献
Eiden, Fritz; Wanner, Klaus Th.
Liebigs Annalen der Chemie, 1984 , # 11 p. 1759 - 1777
反应条件
1: 52 percent / hydroxylamine hydrochloride / ethanol / 0.33 h / Heating
2: 75 percent / hydroxylamine hydrochloride / pyridine / 1 h / Heating
3: PPA / 8 h / 130 - 140 °C
View Scheme
参考文献
Basinski, Wlodzimierz; Jerzmanowska, Zofia
Polish Journal of Chemistry, 1983 , vol. 57, # 4/5/6 p. 471 - 481
反应条件
ammonium acetate
6 h; Reflux;
参考文献
Hemavathi; Naveen; Lokanatha Rai
Indian Journal of Heterocyclic Chemistry, 2011 , vol. 20, # 4 p. 409 - 410
反应条件
1: 68 percent / NH2OH*HCl / ethanol / 0.5 h / Heating
2: 72 percent / Et3N / dimethylformamide / 7 h / Heating
View Scheme
参考文献
Ghosh, Tarun; Saha, Satyajit; Bandyopadhyay, Chandrakanta
Synthesis, 2005 , # 11 art. no. T14704SS, p. 1845 - 1849
反应条件
1: 2 h / 80 - 90 °C
2: 68 percent / NH2OH*HCl / ethanol / 0.5 h / Heating
3: 72 percent / Et3N / dimethylformamide / 7 h / Heating
View Scheme
参考文献
Ghosh, Tarun; Saha, Satyajit; Bandyopadhyay, Chandrakanta
Synthesis, 2005 , # 11 art. no. T14704SS, p. 1845 - 1849
反应条件
1: 75 percent / hydroxylamine hydrochloride / pyridine / 1 h / Heating
2: PPA / 8 h / 130 - 140 °C
View Scheme
参考文献
Basinski, Wlodzimierz; Jerzmanowska, Zofia
Polish Journal of Chemistry, 1983 , vol. 57, # 4/5/6 p. 471 - 481
反应条件
1: 54 percent / 37percent HCl / 0.67 h / Heating
2: 10 percent / hydroxylamine hydrochloride / ethanol / 7 h / Heating
3: PPA / 8 h / 130 - 140 °C
View Scheme
参考文献
Basinski, Wlodzimierz; Jerzmanowska, Zofia
Polish Journal of Chemistry, 1983 , vol. 57, # 4/5/6 p. 471 - 481
