13-羟基亚胺-1-氧杂环十六烷-2-酮合成路线 （共 4 条）
反应条件
1: 40 percent / NaHSO3 / ethanol; H2O / 5 h / Heating 2: 50 percent / 1.) tosylhydrazine, p-toluenesulfonic acid monohydrate, 2.) NaBH3CN / 1.) DMF, sulfolane, 15 min., 2.) cyclohexane, reflux, 4 h View Scheme
参考文献
Mahajan, Jaswant Rai; Araujo, Hugo Clemente
Synthesis, 1980 , # 1 p. 64 - 66
反应条件
hydroxylamine hydrochloride; sodium carbonate in methanol; water
4 h; Reflux;
参考文献
Meng, Xiang-Qing; Zhang, Jian-Jun; Liang, Xiao-Mei; Zhu, Wei-Juan; Dong, Yan-Hong; Wu, Xue-Min; Huang, Jia-Xing; Rui, Chang-Hui; Fan, Xian-Lin; Chen, Fu-Heng; Wang, Dao-Quan
Journal of Agricultural and Food Chemistry, 2009 , vol. 57, # 2 p. 610 - 617
反应条件
hydrogenchloride; n-Butyl nitrite
1.) ethanol, ice temp., 1 h, 2.) room temp., 18 h;
参考文献
Mahajan, Jaswant Rai; Araujo, Hugo Clemente
Synthesis, 1980 , # 1 p. 64 - 66
反应条件
sodium hydrogensulfite in ethanol; water
5 h; Heating;
参考文献
Mahajan, Jaswant Rai; Araujo, Hugo Clemente
Synthesis, 1980 , # 1 p. 64 - 66
