3-(全氟辛基)-2-碘丙醇合成路线 （共 8 条）
反应条件
2,2'-azo-bisisobutyronitrile
参考文献
Shao, Hui; Jiang, Li; Meng, Wei-Dong; Qing, Feng-Ling
Journal of Fluorine Chemistry, 2003 , vol. 124, # 1 p. 89 - 91
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Shao, Hui; Meng, Wei-Dong; Qing, Feng-Ling
Journal of Fluorine Chemistry, 2004 , vol. 125, # 5 p. 721 - 724
反应条件
potassium hydroxide in dichloromethane 1 h; Yield given;
参考文献
Laurent, Philippe; Blancou, Hubert; Commeyras, Auguste
Journal of Fluorine Chemistry, 1993 , vol. 64, # 1-2 p. 125 - 128
→
200112-75-04,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-十七氟十一烷基碘
反应条件
1: 76 percent / LiAlH4 / tetrahydrofuran 2: 76 percent / PPh3; I2; imidazole / CH2Cl2 / 0 - 20 °C View Scheme
参考文献
Vincent, Jean-Marc; Rabion, Alain; Yachandra, Vittal K.; Fish, Richard H.
Angewandte Chemie, International Edition in English, 1997 , vol. 36, # 21 p. 2346 - 2349
Angewandte Chemie, 1997 , vol. 109, p. 2438 - 2440
反应条件
1: 75 percent / AIBN; Bu3SnH / 24 h / 80 °C 2: 90 percent / Jone's reagent / diethyl ether; acetone View Scheme
参考文献
Shao, Hui; Meng, Wei-Dong; Qing, Feng-Ling
Journal of Fluorine Chemistry, 2004 , vol. 125, # 5 p. 721 - 724
反应条件
tri-n-butyl-tin hydride
参考文献
De Campo, Floryan; Lastecoueres, Dominique; Vincent, Jean-Marc; Verlhac, Jean-Baptiste
Journal of Organic Chemistry, 1999 , vol. 64, # 13 p. 4969 - 4971
反应条件
zinc in ethylene glycol T=140°C; 1 h;
参考文献
Journal of Fluorine Chemistry, , vol. 129, # 5 p. 386 - 389
反应条件
phosphorus; sodium hydroxide; iodine
1 h; Heating;
参考文献
Szijjarto, Csongor; Ivanko, Peter; Takacs, Ferenc T.; Szabo, Denes; Rabai, Jozsef
Journal of Fluorine Chemistry, 2008 , vol. 129, # 5 p. 386 - 389
反应条件
zinc in ethylene glycol
T=140°C; 1 h;
参考文献
Szijjarto, Csongor; Ivanko, Peter; Takacs, Ferenc T.; Szabo, Denes; Rabai, Jozsef
Journal of Fluorine Chemistry, 2008 , vol. 129, # 5 p. 386 - 389
