3-(全氟正己基)环氧丙烷合成路线 （共 15 条）
反应条件
1: 95 percent / 1) LiAlH4 / diethyl ether / 10 h / Heating
2: 87 percent / CrO3, conc. H2SO4 / acetone / 3 h / Ambient temperature
View Scheme
参考文献
Moreau,P.; Naji,N.
Journal of Fluorine Chemistry, 1987 , vol. 34, p. 421
反应条件
lithium aluminium tetrahydride in diethyl ether
10 h; Heating;
参考文献
Moreau,P.; Naji,N.
Journal of Fluorine Chemistry, 1987 , vol. 34, p. 421
反应条件
sodium acetate; acetic acid; sodium iodide; zinc in water
2 h; Ambient temperature;
参考文献
Boutevin, B.; Guida-Pietrasanta, F.; Ratsimihety, A.; Caporiccio, G.
Journal of Fluorine Chemistry, 1994 , vol. 68, # 1 p. 71 - 78
反应条件
potassium hydroxide; hydroquinone in neat (no solvent)
T=96°C; 6.5 h;
参考文献
Guery, C.; Viguier, M.; Commeyras, A.
Journal of Fluorine Chemistry, 1987 , vol. 35, p. 497 - 512
反应条件
potassium hydroxide; hydroquinone in melt
T=96°C; 6.5 h; var. conc. of acid, temp., time; KineticsMechanism;
参考文献
Guery, C.; Viguier, M.; Commeyras, A.
Journal of Fluorine Chemistry, 1987 , vol. 35, p. 497 - 512
