3-(全氟正辛基)-1,2-环氧丙烷合成路线 （共 13 条）
反应条件
1: With acetic acid; triethylamine T=95 - 100°C; 10 h; 2: With methanol; potassium hydroxide T=20°C; 2 h;
参考文献
Daikin Industries, Ltd.
Patent: EP1548001 A1, 2005 ;
Location in patent: Page/Page column 7-8 ;
→
92071-84-6(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-十七氟-2-羟基十一烷基)三甲基碘化铵
反应条件
1: methanol / 60 °C
2: acetonitrile / 24 h / 60 °C
View Scheme
参考文献
Padoan, Gennifer; De Givenchy, Elisabeth Taffin; Zaggia, Alessandro; Amigoni, Sonia; Darmanin, Thierry; Conte, Lino; Guittard, Frederic
Soft Matter, 2013 , vol. 9, # 37 p. 8992 - 8999
反应条件
di-tert-octylpyrocatechol; triethylamine
T=100°C; 2 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Cirkva, Vladimir; Ameduri, Bruno; Boutevin, Bernard; Paleta, Oldrich
Journal of Fluorine Chemistry, 1997 , vol. 84, # 1 p. 53 - 61
