1-溴-2,2-二甲基丙烷-1,1-D2合成路线 （共 4 条）
反应条件
tributylphosphine; bromine in N,N-dimethyl-formamide
参考文献
Caulton, Kenneth G.; Chisholm, Malcolm H.; Streib, William E.; Xue, Ziling
Journal of the American Chemical Society, 1991 , vol. 113, # 16 p. 6082 - 6090
反应条件
1: LiAlD4 / diethyl ether
2: 41 percent / PBu3, Br2 / dimethylformamide
View Scheme
参考文献
Bruno,J.W.; Smith,G.M.; Marks,T.J.
Journal of the American Chemical Society, 1986 , vol. 108, p. 40
反应条件
1: 15percent aq. NaOH
2: 88 percent / n-Bu3P, Br2 / dimethylformamide
View Scheme
参考文献
Caulton, Kenneth G.; Chisholm, Malcolm H.; Streib, William E.; Xue, Ziling
Journal of the American Chemical Society, 1991 , vol. 113, # 16 p. 6082 - 6090
反应条件
1: 61 percent / LiAlD4
2: 50 percent / Bu3PBr2
View Scheme
参考文献
Dakternieks, Dainis; Lim, Allan E. K.; Lim, Kieran F.
Chemical Communications, 1999 , # 15 p. 1425 - 1426
