2-甲基-1-丙基溴化镁合成路线 (共 44 条)
反应条件
copper(I) bromide dimethylsulfide complex in tetrahydrofuran T=20°C; 1 h; Yield given. Yields of byproduct given;
参考文献
Gaoni, Yehiel; Tomazic, Alenka
Journal of Organic Chemistry, 1985 , vol. 50, # 16 p. 2948 - 2957
反应条件
N,N,N',N,-tetramethylethylenediamine; iron(III) chloride in tetrahydrofuran T=0°C; 0.5 h;
参考文献
Guerinot, Amandine; Reymond, Sebastien; Cossy, Janine
Angewandte Chemie - International Edition, 2007 , vol. 46, # 34 p. 6521 - 6524
参考文献
Normant; Maitte
Bulletin de la Societe Chimique de France, 1956 , p. 1439
反应条件
Title compound not separated from byproducts.;
参考文献
Kubec, Roman; Velisek, Jan
Journal of Agricultural and Food Chemistry, 2007 , vol. 55, # 9 p. 3491 - 3497
反应条件
o-(PCy2)C6H4-C6H4-(o-OH)C6H4*HBF4; tris(dibenzylideneacetone)dipalladium (0) in tetrahydrofuran T=50°C; 24 h;
参考文献
Ishikawa, Shunpei; Manabe, Kei
Synthesis, 2008 , # 19 art. no. Z16608SS, p. 3180 - 3182
反应条件
[(P{(C6H11)3})2Pd(Cl)2] in tetrahydrofuran T=50°C; 24 h; Inert atmosphere;
参考文献
Ishikawa, Shunpei; Manabe, Kei
Synthesis, 2008 , # 19 art. no. Z16608SS, p. 3180 - 3182
反应条件
in tetrahydrofuran T=-70 - -30°C;
参考文献
Journal of Organic Chemistry, , vol. 52, # 23 p. 5261 - 5266
反应条件
1: in tetrahydrofuran T=-55°C; 1 h; 2: With water; ammonium chloride in tetrahydrofuran
参考文献
US2004/34090 A1, ;
Page/Page column 9 ;
参考文献
Sliwa,H.; Maitte,P.
Bulletin de la Societe Chimique de France, 1962 , p. 369 - 374
反应条件
zinc(II) chloride; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran 1) -25 deg C, 3.5 h, 2) room temperature, 16 h, 3) reflux, 4 h; Further byproducts given. Yields of byproduct given;
参考文献
Rossi, Renzo; Carpita, Adriano; Cossi, Paolo
Tetrahedron, 1992 , vol. 48, # 40 p. 8801 - 8824