6,10-二甲基十一烷-2-醇合成路线 (共 6 条)
反应条件
sodium hydroxide; NiCl2((PPh3)P)2 in isopropyl alcohol
24 h; Heating;
参考文献
Iyer, Suresh; Varghese, Jos P.
Journal of the Chemical Society, Chemical Communications, 1995 , # 4 p. 465 - 466
反应条件
kieselguhr; nickel
T=115 - 125°C; P=36775.4 - 73550.8 Torr; Hydrogenation;
参考文献
Hoffmann-La Roche
Patent: CH219928 , 1941 ;
反应条件
hydrogen; nickel in isopropyl alcohol
T=30°C; P=60754.8 Torr; influence of the concentration of the catalyst; Rate constant;
参考文献
Sul'man, E. M.; Popov, O. S.
Pharmaceutical Chemistry Journal, 1987 , vol. 21, # 11 p. 799 - 802
Khimiko-Farmatsevticheskii Zhurnal, 1987 , vol. 21, # 11 p. 1362 - 1365
反应条件
triethylsilane in dichloromethane
T=20°C; 2 h;
参考文献
Kukovinets; Zainullin; Galin; Odinokov; Tolstikov
Russian Journal of Organic Chemistry, 2000 , vol. 36, # 9 p. 1259 - 1262
反应条件
hydrogen; nickel
various temperatures, various pressures, various times; Product distribution;
参考文献
Gontar', A. I.; Popov, O. S.; Sul'man, E. M.; Ankudinova, T. V.; Sannikov, O. B.; et al.
Pharmaceutical Chemistry Journal, 1983 , vol. 17, # 2 p. 141 - 143
Khimiko-Farmatsevticheskii Zhurnal, 1983 , vol. 17, # 2 p. 197 - 199
参考文献
Asano; Moroe
Yakugaku Zasshi, 1949 , vol. 69, p. 378
Chem.Abstr., 1950 , p. 3080