hydrogen; palladium on activated charcoal in ethanol T=40°C; P=2585.7 Torr; 2 h;
参考文献
Neubert, M. E.; Leung, K.; Jirousek, M. R.; Ezenylimba, M. C.; Sabol-Keast, S.; et al.
Molecular Crystals and Liquid Crystals (1969-1991), 1991 , vol. 197, p. 21 - 41
Neubert, M. E.; Keast, S. S.; Ezenyilimba, M. C.; Greer, P. B.; Jones, W. C.; et al.
Molecular Crystals and Liquid Crystals Science and Technology, Section A: Molecular Crystals and Liquid Crystals, 1993 , vol. 237, p. 47 - 68
1: Ph3P; diisopropyl azodicarboxylate / tetrahydrofuran / 2 h / 20 °C 2: H2; AcOH / Pd(OH)2/C / ethyl acetate / 12 h View Scheme
参考文献
Neubert, M. E.; Leung, K.; Jirousek, M. R.; Ezenylimba, M. C.; Sabol-Keast, S.; et al.
Molecular Crystals and Liquid Crystals (1969-1991), 1991 , vol. 197, p. 21 - 41
ammonium hydroxide in ethanol 1 h; Ambient temperature;
参考文献
Neubert, M. E.; Leung, K.; Jirousek, M. R.; Ezenylimba, M. C.; Sabol-Keast, S.; et al.
Molecular Crystals and Liquid Crystals (1969-1991), 1991 , vol. 197, p. 21 - 41
Neubert, M. E.; Keast, S. S.; Ezenyilimba, M. C.; Greer, P. B.; Jones, W. C.; et al.
Molecular Crystals and Liquid Crystals Science and Technology, Section A: Molecular Crystals and Liquid Crystals, 1993 , vol. 237, p. 47 - 68
Neubert, M. E.; Keast, S. S.; Ezenyilimba, M. C.; Greer, P. B.; Jones, W. C.; et al.
Molecular Crystals and Liquid Crystals Science and Technology, Section A: Molecular Crystals and Liquid Crystals, 1993 , vol. 237, p. 47 - 68
Neubert, M. E.; Leung, K.; Jirousek, M. R.; Ezenylimba, M. C.; Sabol-Keast, S.; et al.
Molecular Crystals and Liquid Crystals (1969-1991), 1991 , vol. 197, p. 21 - 41