2,4,6-trichloro-1,3,5-triazine in N,N-dimethyl-formamide
T=0 - 20°C; 2 h;
参考文献
TAKEDA PHARMACEUTICAL COMPANY LIMITED; TAKEDA SAN DIEGO, INC.
Patent: WO2007/75847 A2, 2007 ;
Location in patent: Page/Page column 109-111 ;
WO 2007/075847 A2
1: With hydrogenchloride; iron in methanol; water
T=20 - 60°C; 2 h;
2: With sodium hydrogencarbonate in tetrahydrofuran; methanol; water; ethyl acetate
参考文献
TAKEDA PHARMACEUTICAL COMPANY LIMITED; TAKEDA SAN DIEGO, INC.
Patent: WO2007/75847 A2, 2007 ;
Location in patent: Page/Page column 109-111 ;
WO 2007/075847 A2
