1-[4-(4-甲基戊-3-烯基)-1-环己-3-烯基]乙酮合成路线 (共 8 条)
反应条件
silica gel
T=20°C; 1 h; Yield given. Yields of byproduct given;
参考文献
Veselovsky, V. V.; Gybin, A. S.; Lozanova, A. V.; Moiseenkov, A. M.; Smit, W. A.; Caple, R.
Tetrahedron Letters, 1988 , vol. 29, # 2 p. 175 - 178
反应条件
silica gel
T=20°C; 1 h; The effect of activation of SiO2 is investigated.; Product distribution;
参考文献
Veselovskii, V. V.; Gybin, A. S.; Lozanova, A. V.; Moiseenkov, A. M.; Smit, V. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 1.1 p. 94 - 100
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , # 1 p. 107 - 113
反应条件
β-Zeolite in dichloromethane
1 h; Heating;
参考文献
Volcho, K. P.; Tatarova, L. E.; Korchagina, D. V.; Salakhutdinov, N. F.; Aul'chenko, I. S.; et al.
Russian Journal of Organic Chemistry, 1994 , vol. 30, # 5.1 p. 683 - 694
Zhurnal Organicheskoi Khimii, 1994 , vol. 30, # 5 p. 641 - 653
反应条件
aluminium amalgam in tetrahydrofuran; water
参考文献
Sharma,S.D. et al.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1976 , vol. 14, p. 1008 - 1009
反应条件
1: NaH / tetrahydrofuran
2: Al-Hg / tetrahydrofuran; H2O
View Scheme
参考文献
Sharma,S.D. et al.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1976 , vol. 14, p. 1008 - 1009
反应条件
1: HCl
2: NaH / tetrahydrofuran
3: Al-Hg / tetrahydrofuran; H2O
View Scheme
参考文献
Sharma,S.D. et al.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1976 , vol. 14, p. 1008 - 1009
反应条件
phosphoric acid
T=100°C; 3 h; also other substituted-cyclohexene derivatives, var. kind and amount of catalyst, temp., and time; Product distribution;
参考文献
Kron, A. A.; Burdin, E. A.; Fedotova, Z. M.; Novikov, N. A.
Russian Journal of Organic Chemistry, 1994 , vol. 30, # 7.1 p. 1035 - 1038
Zhurnal Organicheskoi Khimii, 1994 , vol. 30, # 7 p. 979 - 982
反应条件
sodium hydride in tetrahydrofuran; dimethyl sulfoxide
参考文献
Sharma,S.D. et al.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1976 , vol. 14, p. 1008 - 1009