2,3-二氯-N-苯基马来酰亚胺合成路线 （共 13 条）
反应条件
1: 77 percent / sodium azide / acetonitrile / 5 h / 0 °C 2: 32 percent / chlorobenzene / 2 h / 100 °C View Scheme
参考文献
Moore,H.W.; Hernandez,L.; Kunert,D.M.
Journal of the American Chemical Society, 1981 , vol. 103, p. 1769
反应条件
in acetic acid
T=85 - 108°C; 2 h;
参考文献
Nagiev
Russian Journal of Organic Chemistry, 2012 , vol. 48, # 3 p. 469 - 472
反应条件
thionyl chloride in pyridine; dichloromethane
Chlorination; 8 h; Heating;
参考文献
Hanaineh-Abdelnour, Leila; Bayyuk, Shibly; Theodorie, Rima
Tetrahedron, 1999 , vol. 55, # 40 p. 11859 - 11870
反应条件
1: in acetone
T=55°C; 1 h;
2: With nickel sulphate; acetic anhydride; triethylamine in acetone
T=80°C; 2 h;
3: With pyridine; thionyl chloride
T=0 - 85°C; 3 h;
参考文献
Wu, Peng; Hu, Yongzhou
Synthetic Communications, 2009 , vol. 39, # 1 p. 70 - 84
反应条件
sodium acetate; acetic anhydride
2 h; Reflux;
参考文献
Sortino; Garibotto; Cechinel Filho; Gupta; Enriz; Zacchino
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 9 p. 2823 - 2834
反应条件
1: chloroform / 1 h / 20 °C
2: sodium acetate; acetic anhydride / 2 h / Reflux
View Scheme
参考文献
Sortino; Garibotto; Cechinel Filho; Gupta; Enriz; Zacchino
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 9 p. 2823 - 2834
反应条件
1: in diethyl ether
Heating;
2: With sodium acetate; acetic acid
Heating;
参考文献
Mao, Yingqun; Maley, Iain; Watson, William H.
Journal of Chemical Crystallography, 2005 , vol. 35, # 5 p. 385 - 403
反应条件
phosphorus pentachloride; trichlorophosphate
参考文献
Kauder
Journal fuer Praktische Chemie (Leipzig), 1885 , vol. <2> 31, p. 4,6, 8
反应条件
1: Ac2O
2: 87 percent / SOCl2; pyridine / 1.67 h
View Scheme
参考文献
Gaina, Constantin
Revue Roumaine de Chimie, 2005 , vol. 50, # 7-8 p. 601 - 607
参考文献
Anschuetz; Beavis
Justus Liebigs Annalen der Chemie, 1897 , vol. 295, p. 32
