反应条件
1: 77 percent / tetrahydrofuran 2: NaIO4 3: NH2OH*HCl, pyridine 4: pyridine 5: LiAlH4 / diethyl ether 6: 1.) HCl, H2O, 2.) HBr / 1.) MeOH, reflux, 2.) 10 deg C 7: KOH, H2O / methanol 8: HClO4 / CHCl3 / 60 °C 9: 1.) Et3N, 2.) pyridine / 1.) CHCl3 10: 1.) dil. HCl, 2.) H2, HCl / 1.) Pd/C, 2.) Pd/C / 1.) MeOH, reflux, 2.) MeOH View Scheme
参考文献
Buchanan; MacLean; Paulsen; Wightman
Journal of the Chemical Society - Series Chemical Communications, 1983 , vol. No. 9, p. 486 - 488
